Synlett

Issue 20 · December 2014

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2819
Yayla, Hatice G.; Knowles, Robert R.:
Proton-Coupled Electron Transfer in Organic Synthesis: Novel Homolytic Bond Activations and Catalytic Asymmetric Reactions with Free Radicals

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2827
Lin, Chin-Yin; Chein, Rong-Jie:
Lithiation of a Silyl Ether: Anionic Si→C Alkyl Migration

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account
2831
Sada, Mutsumi; Uchiyama, Masanobu; Matsubara, Seijiro:
Design of Molecular Transformations Based on the Concerted Function of Two Zinc Atoms in Bis(iodozincio)methane

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2842
Bernadat, Guillaume; Masson, Geraldine:
Enamide Derivatives: Versatile Building Blocks for Highly Functionalized α,β-Substituted Amines

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letter
2868
Grosso, Carla; Lemos, Américo; Pinho e Melo, Teresa M. V. D.:
Conjugate Addition of Pyrazoles to Halogenated Nitroso- and Azoalkenes: A New Entry to Novel Bis(pyrazol-1-yl)methanes

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2873
Cancogni, Damiano; Lay, Luigi:
Exploring Glycosylation Reactions under Continuous-Flow Conditions

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2879
Chavan, Subhash P.; Chavan, Prakash N.; Lasonkar, Pradeep B.; Khairnar, Lalit B.; Kadam, Appasaheb L.:
A Facile and Convenient Synthesis of (±)-Biotin via MgCl₂/Et₃N-Mediated C–C Coupling and Mitsunobu Reaction

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2883
Feuillastre, Sophie; Piva, Olivier:
Total Synthesis of (+)-Guaymasol

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2887
Revu, Omkar; Prasad, Kavirayani R.:
An Expeditious Asymmetric Synthesis of the Polyketide Unit Present in HIV-Inhibitory Depsipeptides Aetheramide A and B

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2891
Maresh, Justin J.; Ralko, Arthur A.; Speltz, Tom E.; Burke, James L.; Murphy, Casey M.; Gaskell, Zachary; Girel, JoAnn K.; Terranova, Erin; Richtscheidt, Conrad; Krzeszowiec, Mark:
Chemoselective Zinc/HCl Reduction of Halogenated β-Nitrostyrenes: Synthesis of Halogenated Dopamine Analogues

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2895
Wang, Dawei; Ge, Bingyang; Du, Liyong; Miao, Hongyan; Ding, Yuqiang:
Synthesis of Aryl- and Alkylquinones through Rhodium-Catalyzed C–C Coupling under Mild Conditions

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2899
Li, Zhengning; Feng, Yunyun; Li, Zengchang; Jiang, Lan:
Copper-Catalyzed Three-Component Tandem Reactions for the Synthesis of β-Carboalkoxy-γ-lactams

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2903
Hajipour, Abdol Reza; Karimzadeh, Morteza; Ghorbani, Sirous:
Selective Azidation of Aryl Halides to Aryl Azides Promoted by Proline and CuFeO₂

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2908
Liu, Guifeng; Jin, Can; Wu, Guomin:
Cu(II)/TBAI-Catalyzed Esterification of Acid Hydrazides via C(sp³)–H Oxidative Coupling

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2913
Xu, Zian; Ge, Jingying; Wang, Tianchi; Luo, Ting; Liu, Hongwei; Yu, Xinhong:
Highly Stereoselective Synthesis of 2-Aminobenzylidene Derivatives by a Convergent 3-Component Approach

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2918
Adib, Mehdi; Bayanati, Maryam; Soheilizad, Mehdi; Ghazvini, Helia Janatian; Tajbakhsh, Mahmood; Amanlou, Massoud:
A Simple Synthesis of Alkyl 2-Aminobenzo[b]thiophene-3-carboxylates via an Unexpected Dehydrogenation of Alkyl 2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylates

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2923
Attoui, Mariam; Vatèle, Jean-Michel:
TEMPO/NBu₄Br-Catalyzed Selective Alcohol Oxidation with Periodic Acid

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2928
Zhang, Pengbo; Xu, Jian; Gao, Yuzhen; Li, Xueqin; Tang, Guo; Zhao, Yufen:
Synthesis of Diarylmethanes through Palladium-Catalyzed Coupling of Benzylic Phosphates with Arylsilanes

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2933
Kamihigashi, Shun; Shibata, Naoatsu; Sakaguchi, Satoshi:
Cu-Catalyzed Asymmetric Conjugate Addition of Dialkylzincs to Enones Using a (±)-trans-1,2-Cyclohexanediamine-Based Bis(NHC) Derived from l-Leucinol

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2938
Tu, Yahui; Zhang, Yi; Xu, Sheng; Zhang, Zhaoguo; Xie, Xiaomin:
Cyanation of Unactivated Aryl Chlorides and Aryl Mesylates Catalyzed by Palladium and Hemilabile MOP-Type Ligands

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2943
Schmidt, Bernd; Riemer, Martin; Schilde, Uwe:
Chroman-4-ones via Microwave-Promoted Domino Claisen Rearrangement–Oxa-Michael Addition: Synthesis of Tabchromones A and B

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2947
Lefranc, Alice; Guénée, Laure; Goncalves-Contal, Sylvie; Alexakis, Alexandre:
Direct Organocatalytic Construction of Bicyclo[3.2.1]octanes by Domino Michael/Aldol Reaction with β,γ-Unsaturated 1,2-Keto Amides

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2953
Tanda, Kazuhiro; Toyao, Atsushi; Watanabe, Akiko; Sakamoto, Masanori; Yamasaki, Tetsuo:
Magnesium-Coordinated Chelation Control in 1,3-Dipolar Cycloaddition of Chiral α-Alkoxymethyl Ether Nitrile Oxide: Application to the Synthesis of (–)/(–)-cis-Clausenamide

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2957
Hejmanowska, Joanna; Dzięgielewski, Marek; Kowalczyk, Dorota; Albrecht, Łukasz:
Organocatalytic Enantioselective Approach to Spirocyclic Δ^β,γ-Butenolides

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spotlight
2962
Lugiņina, Jevgeņija:
Sulfur Dioxide in the Past Decade
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2964
Yang, Li-Fen:
Heterocyclic Ketene Aminals
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Synlett

Proton-Coupled Electron Transfer in Organic Synthesis: Novel Homolytic Bond Activations and Catalytic Asymmetric Reactions with Free Radicals

Lithiation of a Silyl Ether: Anionic Si→C Alkyl Migration

Design of Molecular Transformations Based on the Concerted Function of Two Zinc Atoms in Bis(iodozincio)methane

Enamide Derivatives: Versatile Building Blocks for Highly Functionalized α,β-Substituted Amines

Conjugate Addition of Pyrazoles to Halogenated Nitroso- and Azoalkenes: A New Entry to Novel Bis(pyrazol-1-yl)methanes

Exploring Glycosylation Reactions under Continuous-Flow Conditions

A Facile and Convenient Synthesis of (±)-Biotin via MgCl₂/Et₃N-Mediated C–C Coupling and Mitsunobu Reaction

Total Synthesis of (+)-Guaymasol

An Expeditious Asymmetric Synthesis of the Polyketide Unit Present in HIV-Inhibitory Depsipeptides Aetheramide A and B

Chemoselective Zinc/HCl Reduction of Halogenated β-Nitrostyrenes: Synthesis of Halogenated Dopamine Analogues

Synthesis of Aryl- and Alkylquinones through Rhodium-Catalyzed C–C Coupling under Mild Conditions

Copper-Catalyzed Three-Component Tandem Reactions for the Synthesis of β-Carboalkoxy-γ-lactams

Selective Azidation of Aryl Halides to Aryl Azides Promoted by Proline and CuFeO₂

Cu(II)/TBAI-Catalyzed Esterification of Acid Hydrazides via C(sp³)–H Oxidative Coupling

Highly Stereoselective Synthesis of 2-Aminobenzylidene Derivatives by a Convergent 3-Component Approach

A Simple Synthesis of Alkyl 2-Aminobenzo[b]thiophene-3-carboxylates via an Unexpected Dehydrogenation of Alkyl 2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylates

TEMPO/NBu₄Br-Catalyzed Selective Alcohol Oxidation with Periodic Acid

Synthesis of Diarylmethanes through Palladium-Catalyzed Coupling of Benzylic Phosphates with Arylsilanes

Cu-Catalyzed Asymmetric Conjugate Addition of Dialkylzincs to Enones Using a (±)-trans-1,2-Cyclohexanediamine-Based Bis(NHC) Derived from l-Leucinol

Cyanation of Unactivated Aryl Chlorides and Aryl Mesylates Catalyzed by Palladium and Hemilabile MOP-Type Ligands

Chroman-4-ones via Microwave-Promoted Domino Claisen Rearrangement–Oxa-Michael Addition: Synthesis of Tabchromones A and B

Direct Organocatalytic Construction of Bicyclo[3.2.1]octanes by Domino Michael/Aldol Reaction with β,γ-Unsaturated 1,2-Keto Amides

Magnesium-Coordinated Chelation Control in 1,3-Dipolar Cycloaddition of Chiral α-Alkoxymethyl Ether Nitrile Oxide: Application to the Synthesis of (–)/(–)-cis-Clausenamide

Organocatalytic Enantioselective Approach to Spirocyclic Δ^β,γ-Butenolides

Sulfur Dioxide in the Past Decade

Heterocyclic Ketene Aminals