Synthesis

Issue 04 · February 2019

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table of contents
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review
787
Trushkov, Igor V.; Uchuskin, Maxim G.; Abaev, Vladimir T.; Serdyuk, Olga V.:
Indolylvinyl Ketones: Building Blocks for the Synthesis of Natural Products and Bioactive Compounds

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short review
816
Leonardi, Marco; Estévez, Verónica; Villacampa, Mercedes; Menéndez, J. Carlos:
The Hantzsch Pyrrole Synthesis: Non-conventional Variations and Applications of a Neglected Classical Reaction
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829
Palmieri, Alessandro; Petrini, Marino:
Recent Advances in the Synthesis of Unsymmetrical Bisindolylmethane Derivatives

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psp
842
Morales-Chamorro, Maricela; Vázquez, Alfredo:
A Facile Synthesis of N-Boc-azocan-5-one

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paper
848
Sokolov, Andriy; Golovach, Sergey; Kozlinsky, Ihor; Dolia, Krystyna; Tolmachev, Andrey A.; Kuchkovska, Yuliya; Grygorenko, Oleksandr O.:
Diastereoselective Synthesis of Cyclic sp³-Enriched cis-β-Alkoxysulfonyl Chlorides

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859
Kim, Hyokwon; Zong, Kyukwan:
A Convenient Synthesis of Benzo[1,2-b:6,5-b′:3,4-c′′]trithiophenes Starting from Thiophene

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PDF (360 kb)
865
Ndimba, A. Ngo; Roisnel, T.; Argouarch, G.; Lalli, C.:
Harvesting New Chiral Phosphotriesters by Phosphorylation of BINOL and Parent Bis-phenols

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874
Xue, Dengqi; Xue, Yijie; Yu, Haihua; Shao, Liming:
Metal-Free Radical Cyclization of Vinyl Isocyanides with Alkanes: Synthesis of 1-Alkylisoquinolines

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885
Kim, Sonhwan; Lee, Won Koo; Ha, Hyun-Joon:
Asymmetric Synthesis of cis-5-(Aminomethyl)-3-(4-methoxyphenyl)dihydrofuran-2(3H)-one

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889
Zhang, Xing; Du, Cong; Zhang, He; Li, Xiao-Cai; Wang, Yun-Long; Niu, Jun-Long; Song, Mao-Ping:
Metal-Free Blue-Light-Mediated Cyclopropanation of Indoles by Aryl(diazo)acetates

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PDF (276 kb)

Supplementary Material

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899
Zhu, Yuanyuan; Zhao, Shuang; Zhang, Minli; Song, Xixi; Chang, Junbiao:
Diastereoselective Synthesis of Spirobarbiturate-Cyclopropanes through Organobase-Mediated Spirocyclopropanation of Barbiturate-Based Olefins with Benzyl Chlorides

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PDF (294 kb)

Supplementary Material

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907
Formánek, Bedřich; Šimek, Michal; Kamlar, Martin; Císařová, Ivana; Veselý, Jan:
Organocatalytic Allylic Amination of Morita–Baylis–Hillman Carbonates

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921
Ramkumar, Rajagopal; Chandrasekaran, Srinivasan:
Catalyst-Free, Metal-Free, and Chemoselective Transamidation of Activated Secondary Amides
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PDF (228 kb)

Supplementary Material

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933
Lessi, Marco; Panattoni, Alessandro; Guglielmero, Luca; Minei, Pierpaolo; Bellina, Fabio:
Imidazole-Fused Enediynes by Selective C5–C4 Alkynylations of 4,5-Dibromoimidazoles

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Supplementary Material

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944
Zheng, Xiu-An; Kong, Rui; Huang, Hua-Shan; Wei, Jing-Ying; Chen, Ji-Zong; Gong, Shan-Shan; Sun, Qi:
Hafnium Triflate as a Highly Potent Catalyst for Regio- and Chemoselective Deprotection of Silyl Ethers

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Supplementary Material

Supporting Information (PDF)
953
deLong, Mitchell A.; Sturdivant, Jill M.:
Asymmetric Synthesis of Netarsudil: A New Therapeutic for Open-Angle Glaucoma

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Supplementary Material

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960
Parveen, Iram; Ahmed, Naseem:
A Route to Highly Functionalized Stereospecific trans-Aminated Aurones from 3-Bromoflavones with Aniline and N-Phenylurea via a Domino Aza-Michael Ring Opening and Cyclization Reactions

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971
Glachet, Thomas; Franck, Xavier; Reboul, Vincent:
Late-Stage Sulfoximination: Improved Synthesis of the Anticancer Drug Candidate Atuveciclib

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976
Bartuschat, Amelie L.; Hegmann, Nina; Heinrich, Markus R.:
Synthesis of Fmoc- and Boc-Protected (2S,5S)- and (2R,5R)-5-Aminomethylprolines

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Synthesis

Linked PDF of Table of Contents

Indolylvinyl Ketones: Building Blocks for the Synthesis of Natural Products and Bioactive Compounds

The Hantzsch Pyrrole Synthesis: Non-conventional Variations and Applications of a Neglected Classical Reaction

Recent Advances in the Synthesis of Unsymmetrical Bisindolylmethane Derivatives

A Facile Synthesis of N-Boc-azocan-5-one

Diastereoselective Synthesis of Cyclic sp³-Enriched cis-β-Alkoxysulfonyl Chlorides

A Convenient Synthesis of Benzo[1,2-b:6,5-b′:3,4-c′′]trithiophenes Starting from Thiophene

Harvesting New Chiral Phosphotriesters by Phosphorylation of BINOL and Parent Bis-phenols

Metal-Free Radical Cyclization of Vinyl Isocyanides with Alkanes: Synthesis of 1-Alkylisoquinolines

Asymmetric Synthesis of cis-5-(Aminomethyl)-3-(4-methoxyphenyl)dihydrofuran-2(3H)-one

Metal-Free Blue-Light-Mediated Cyclopropanation of Indoles by Aryl(diazo)acetates

Diastereoselective Synthesis of Spirobarbiturate-Cyclopropanes through Organobase-Mediated Spirocyclopropanation of Barbiturate-Based Olefins with Benzyl Chlorides

Organocatalytic Allylic Amination of Morita–Baylis–Hillman Carbonates

Catalyst-Free, Metal-Free, and Chemoselective Transamidation of Activated Secondary Amides

Imidazole-Fused Enediynes by Selective C5–C4 Alkynylations of 4,5-Dibromoimidazoles

Hafnium Triflate as a Highly Potent Catalyst for Regio- and Chemoselective Deprotection of Silyl Ethers

Asymmetric Synthesis of Netarsudil: A New Therapeutic for Open-Angle Glaucoma

A Route to Highly Functionalized Stereospecific trans-Aminated Aurones from 3-Bromoflavones with Aniline and N-Phenylurea via a Domino Aza-Michael Ring Opening and Cyclization Reactions

Late-Stage Sulfoximination: Improved Synthesis of the Anticancer Drug Candidate Atuveciclib

Synthesis of Fmoc- and Boc-Protected (2S,5S)- and (2R,5R)-5-Aminomethylprolines