Synlett

Issue 01 · January 2010

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Zanda, Matteo:
SYNFORM ISSUE 2010/01
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Sohtome, Yoshihiro; Nagasawa, Kazuo:
The Design of Chiral Double Hydrogen Bonding Networks and Their Applications to Catalytic Asymmetric Carbon-Carbon and Carbon-Oxygen Bond-Forming Reactions

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23
Banfi, Luca; Riva, Renata; Basso, Andrea:
Coupling Isocyanide-Based Multicomponent Reactions with Aliphatic or Acyl Nucleophilic Substitution Processes

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letter
42
Dekaris, Vjekoslav; Reissig, Hans-Ulrich:
Stereocontrolled Synthesis of Enantiopure Polyhydroxylated Azetidines via 1,2-Oxazines

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47
Dekaris, Vjekoslav; Bressel, Bettina; Reissig, Hans-Ulrich:
Acid-Mediated Transformations of Enantiopure 3,6-Dihydro-2H-1,2-oxazines into Functionalised Aminotetrahydrofuran Derivatives

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51
Yadav, J. S.; Rao, K. V. Raghavendra; Ravindar, K.; Reddy, B. V. Subba:
Total Synthesis of (+)-Aculeatin D and (+)-6-epi-Aculeatin D

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55
Cebrián, C.; de Cózar, A.; Prieto, P.; Díaz-Ortiz, A.; de la Hoz, A.; Carrillo, J. R.; Rodriguez, A. M.; Montilla, F.:
Microwave-Assisted Stille Reactions as a Powerful Tool for Building Polyheteroaryl Systems Bearing a (1H)-1,2,4-Triazole Moiety

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61
Hummel, Johanna; Winter, Andreas; Baumgaertel, Anja; Risch, Nikolaus; Schubert, Ulrich S.:
New Ditopic Ligands Containing 2,2′:6′,2′′-Terpyridine and a Rigid U-/S-Shaped Terpyridine

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67
Yedukondalu, M.; Ravikanth, M.:
Borylated Thiaporphyrin Building Blocks for the Synthesis of Unsymmetrical Phenyl-Bridged Porphyrin Dyads

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73
Shevchuk, Michael V.; Sorochinsky, Alexander E.; Khilya, Volodymyr P.; Romanenko, Vadim D.; Kukhar, Valery P.:
Utilization of Aminophosphonates in the Petasis Boronic Acid Mannich Reaction

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77
Funicello, Maria; Laboragine, Valeria; Pandolfo, Rocco; Spagnolo, Piero:
A New Entry to Benzo[4,5]furo[3,2-b]pyridines via N-(Benzofuran-3-yl)iminophosphorane

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81
Schweizer, Stefan A.; Bach, Thorsten:
Regioselective Pd(0)-Catalyzed Hiyama Cross-Coupling Reactions at Dihalo-Substituted Heterocycles

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85
Banfi, Luca; Basso, Andrea; Casuscelli, Francesco; Guanti, Giuseppe; Naz, Farah; Riva, Renata; Zito, Paola:
Synthesis of Novel Isochromene Derivatives by Tandem Ugi Reaction/Nucleophilic Substitution

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89
Calitree, Brandon D.; Detty, Michael R.:
Novel Rhodamine Dyes via Suzuki Coupling of Xanthone Triflates with Arylboroxins

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93
Mase, Nobuyuki; Kitagawa, Norihiko; Takabe, Kunihiko:
Protection-, Salt-, and Metal-Free Syntheses of [n]-Shogaols by Use of Dimethylammonium Dimethyl Carbamate (DIMCARB) without Protecting Groups

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97
Tsuchikama, Kyoji; Kasagawa, Mitsugu; Endo, Kohei; Shibata, Takanori:
Sequential Catalytic Reactions for the Synthesis of Benzofulvenes Using an Iridium Complex with Dual Function

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101
Yang, Xiaobo; Liu, Hongxia; Fu, Hua; Qiao, Renzhong; Jiang, Yuyang; Zhao, Yufen:
Efficient Copper-Catalyzed Synthesis of 4-Aminoquinazoline and 2,4-Diaminoquinazoline Derivatives

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107
O’Neil, Gregory W.; Black, Matthew J.:
A Synthesis of the C₃-C₁₅ Fragment of the Archazolids

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111
Lai, Jiun-Ting; Yang, Yu-Ju; Lin, Jian-Hung; Yang, Ding-Yah:
Fluorescence Redox Switches Based on the Opening and Closing of an Oxazabicyclic Ring

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115
Resende, Diana I. S. P.; Oliva, Cristina G.; Silva, Artur M. S.; Almeida Paz, Filipe A.; Cavaleiro, José A. S.:
Domino Multicomponent Michael-Michael-Aldol Reactions under Phase-Transfer Catalysis: Diastereoselective Synthesis of Pentasubstituted Cyclohexanes

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119
Rueping, Magnus; Nachtsheim, Boris J.:
Asymmetric Brønsted Acid Catalyzed Nucleophilic Addition to in situ Generated Chiral N-Acyliminium Ions

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123
Moghaddam, Firouz Matloubi; Taheri, Salman; Mirjafary, Zohreh; Saeidian, Hamdollah:
New Entry to Bridged Pentacyclic Indolyltetrahydroisoquinoline Skeleton via Tandem S-Alkylation and Intramolecular C-Alkylation

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128
Ay, Sefer; Gérard, Emilie M. C.; Shi, Min; Bräse, Stefan:
The Domino Oxa-Michael-Aldol-Reaction Reinvestigated: A New P-Based Organocatalyst for Xanthenone Scaffolds

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131
Pinho, Pedro; Pelcman, Mikael; Agback, Tatiana; Samuelsson, Bertil:
Asymmetric Synthesis of α- and β-Benzylhydroxy-γ-butyrolactones

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134
Guizzetti, Stefania; Benaglia, Maurizio; Biaggi, Cinzia; Celentano, Giuseppe:
A Convenient, Highly Stereoselective, Metal-Free Synthesis of Chiral Amines

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137
Thies, Sarah; Kazmaier, Uli:
Vinylepoxides as Versatile Substrates for Allylations of Amino Acids and Peptides

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142
Shing, Tony K. M.; Cheng, Hau M.:
The Structure and Stereochemistry of Gabosine K: Syntheses of 7-O-Acetylstreptol and 7-O-Acetyl-1-epi-streptol

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145
Bonifácio, Vasco D. B.; González-Bello, Concepción; Rzepa, Henry S.; Prabhakar, Sundaresan; Lobo, Ana M.:
Chiral Aziridination of Olefins Using a Chiral Sulfinamide as the Nitrogen Source

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150
Nawaz, Muhammad; Ibad, Muhammad Farooq; Abid, Obaid-Ur-Rahman; Khera, Rasheed Ahmad; Villinger, Alexander; Langer, Peter:
Synthesis of Functionalized p-Terphenyls Based on Site-Selective Suzuki Cross-Coupling Reactions of Bis(triflates) of 2,5-Dihydroxybenzoate

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153
Barthelon, Anaëlle; Legoff, Xavier-Frédéric; El Kaim, Laurent; Grimaud, Laurence:
Four-Component Synthesis of Imidazolinium-Fused Heterocycles from Ugi-Smiles Couplings

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158
Fernandes, Rodney A.; Ingle, Arun B.:
Total Synthesis of (+)-Cephalosporolide E and (-)-Cephalosporolide F en route to Bassianolone

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spotlight
161
Crucho, Carina I. C.:
Ytterbium Triflate: A Green Catalyst
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163
Wang, Qiao-Feng:
9-Amino-9-Deoxyepicinchona Alkaloids
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addenda and errata
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Synthesis of Functionalized p-Terphenyls Based on Site-Selective Suzuki Cross-Coupling Reactions of Bis(triflates) of 2,5-Dihydroxybenzoate
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Synlett

Editorial

SYNFORM ISSUE 2010/01

The Design of Chiral Double Hydrogen Bonding Networks and Their Applications to Catalytic Asymmetric Carbon-Carbon and Carbon-Oxygen Bond-Forming Reactions

Coupling Isocyanide-Based Multicomponent Reactions with Aliphatic or Acyl Nucleophilic Substitution Processes

Stereocontrolled Synthesis of Enantiopure Polyhydroxylated Azetidines via 1,2-Oxazines

Acid-Mediated Transformations of Enantiopure 3,6-Dihydro-2H-1,2-oxazines into Functionalised Aminotetrahydrofuran Derivatives

Total Synthesis of (+)-Aculeatin D and (+)-6-epi-Aculeatin D

Microwave-Assisted Stille Reactions as a Powerful Tool for Building Polyheteroaryl Systems Bearing a (1H)-1,2,4-Triazole Moiety

New Ditopic Ligands Containing 2,2′:6′,2′′-Terpyridine and a Rigid U-/S-Shaped Terpyridine

Borylated Thiaporphyrin Building Blocks for the Synthesis of Unsymmetrical Phenyl-Bridged Porphyrin Dyads

Utilization of Aminophosphonates in the Petasis Boronic Acid Mannich Reaction

A New Entry to Benzo[4,5]furo[3,2-b]pyridines via N-(Benzofuran-3-yl)iminophosphorane

Regioselective Pd(0)-Catalyzed Hiyama Cross-Coupling Reactions at Dihalo-Substituted Heterocycles

Synthesis of Novel Isochromene Derivatives by Tandem Ugi Reaction/Nucleophilic Substitution

Novel Rhodamine Dyes via Suzuki Coupling of Xanthone Triflates with Arylboroxins

Protection-, Salt-, and Metal-Free Syntheses of [n]-Shogaols by Use of Dimethylammonium Dimethyl Carbamate (DIMCARB) without Protecting Groups

Sequential Catalytic Reactions for the Synthesis of Benzofulvenes Using an Iridium Complex with Dual Function

Efficient Copper-Catalyzed Synthesis of 4-Aminoquinazoline and 2,4-Diaminoquinazoline Derivatives

A Synthesis of the C₃-C₁₅ Fragment of the Archazolids

Fluorescence Redox Switches Based on the Opening and Closing of an Oxazabicyclic Ring

Domino Multicomponent Michael-Michael-Aldol Reactions under Phase-Transfer Catalysis: Diastereoselective Synthesis of Pentasubstituted Cyclohexanes

Asymmetric Brønsted Acid Catalyzed Nucleophilic Addition to in situ Generated Chiral N-Acyliminium Ions

New Entry to Bridged Pentacyclic Indolyltetrahydroisoquinoline Skeleton via Tandem S-Alkylation and Intramolecular C-Alkylation

The Domino Oxa-Michael-Aldol-Reaction Reinvestigated: A New P-Based Organocatalyst for Xanthenone Scaffolds

Asymmetric Synthesis of α- and β-Benzylhydroxy-γ-butyrolactones

A Convenient, Highly Stereoselective, Metal-Free Synthesis of Chiral Amines

Vinylepoxides as Versatile Substrates for Allylations of Amino Acids and Peptides

The Structure and Stereochemistry of Gabosine K: Syntheses of 7-O-Acetylstreptol and 7-O-Acetyl-1-epi-streptol

Chiral Aziridination of Olefins Using a Chiral Sulfinamide as the Nitrogen Source

Synthesis of Functionalized p-Terphenyls Based on Site-Selective Suzuki Cross-Coupling Reactions of Bis(triflates) of 2,5-Dihydroxybenzoate

Four-Component Synthesis of Imidazolinium-Fused Heterocycles from Ugi-Smiles Couplings

Total Synthesis of (+)-Cephalosporolide E and (-)-Cephalosporolide F en route to Bassianolone

Ytterbium Triflate: A Green Catalyst

9-Amino-9-Deoxyepicinchona Alkaloids

Synthesis of Functionalized p-Terphenyls Based on Site-Selective Suzuki Cross-Coupling Reactions of Bis(triflates) of 2,5-Dihydroxybenzoate