Synthesis

Issue 19 · December 2005

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3183
Reetz, Manfred T.; Li, Xiaoguang:
Rhodium-Catalyzed Enantioselective Hydrogenation of β,β-Disubstituted α-Acetamido Acrylates Using Cheap Monodentate P-Ligands

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3186
Bégis, Guillaume; Sheppard, Tom D.; Cladingboel, David E.; Motherwell, William B.; Tocher, Derek A.:
Synthesis of Enantiopure Aminocyclopropanes by Diastereoselective Addition of a Chiral Amino Substituted Organozinc Carbenoid to Alkenes

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3189
Ullah, Ehsan; Langer, Peter:
Synthesis of Pyran-2-ones by Reaction of 1,1-Bis(trimethylsilyloxy)ketene Acetals with 3-Silyloxyalk-2-en-1-ones

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3191
Shimasaki, Yasuharu; Kiyota, Hiromasa; Sato, Minoru; Kuwahara, Shigefumi:
Facile Synthesis of (S)-Gizzerosine - A Potent Inducer of Gizzard Erosion in Chicks - Using Successive Zinc-Mediated and Palladium-Catalyzed Coupling Reactions

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3193
Quesada, Ernesto; Taylor, Richard J. K.:
Tandem Horner-Wadsworth-Emmons Olefination/Claisen Rearrangement/Hydrolysis Sequence: Remarkable Acceleration in Water with Microwave Irradiation

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3196
Fox, Martin E.; Gerlach, Arne; Lennon, Ian C.; Meek, Graham; Praquin, Céline:
A Convenient and Scaleable Synthesis of 11,12-Diamino-9,10-dihydro-9,10-ethanoanthracene and Its Enantiomers

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3199
Mak, S. Y. Frankie; Curtis, Neil R.; Payne, Andrew N.; Congreve, Miles S.; Francis, Craig L.; Burton, Jonathan W.; Holmes, Andrew B.:
A Synthesis of (+)-Obtusenyne

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paper
3202
Castro, Mª Angeles; Miguel del Corral, José Mª; Gordaliza, Marina; García, Pablo A.; Gamito, Ana Mª; Gualberto, Simone A.; Batista, Ronan; San Feliciano, Arturo:
A Novel Synthetic Route to Cytotoxic 1,4-Anthraquinones from 1,4-Benzoquinones

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3209
Hartung, Ryan E.; Paquette, Leo A.:
Development of a Generic Stereocontrolled Pathway to Fully Hydroxylated Spirocarbocyclic Nucleosides as a Prelude to RNA Targeting

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3219
Bourque, Elyse; Kocienski, Philip J.; Stocks, Michael; Yuen, Josephine:
Synthesis of the C14-C28 Fragment of Tetronasin

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3225
Paterson, Ian; Anderson, Edward A.; Dalby, Stephen M.:
Synthesis of the C₁-C₂₁ Southern Hemisphere of the Originally Proposed Structure of Spirastrellolide A

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3229
Willis, Michael C.; Brace, Gareth N.; Holmes, Ian P.:
Efficient Palladium-Catalysed Enamide Synthesis from Enol Triflates and Enol Tosylates

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3235
Helliwell, Madeleine; Thomas, Eric J.; Whitehouse, Darren L.:
A Diels-Alder Approach to Potential Precursors of Polyhydroxylated Dihydroagarofurans: A Ring-Opening/Ring-Closing Rearrangement

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3239
Enders, Dieter; Breuer, Irene; Drosdow, Eugen:
Asymmetric Synthesis of 4′-epi-Trachycladines A and B

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3245
Krafft, Eva A.; Kurt, Anke; Maier, Axel; Thomas, Andrew W.; Zimmerli, Daniel:
A Straightforward and Efficiently Scaleable Synthesis of Novel Racemic 4-Substituted-2,8-diazaspiro[4.5]decan-1-one Derivatives

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3253
Barrett, Anthony G. M.; Frederiksen, Mathias U.:
Studies on the Transesterification and Macrolactonization of 2-Pyridyl Esters by Intramolecular N-Alkylation or Metal Ion Coordination

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3257
Lygo, Barry; Hirst, David J.:
IMDA Reactions of β,δ-Diketoester-Substituted 1,7,9-Undecatrienes: Application in the Formal Synthesis of Solanapyrone D

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3263
Newton, Rebecca; Marsden, Stephen P.:
Efficient Synthesis of Quaternary α-Hydroxy Acids by Alkylation of α-Ketoamide-Derived Dienediolates

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3271
Aldous, David J.; Drew, Michael G. B.; Draffin, William N.; Hamelin, Estelle M.-N.; Harwood, Laurence M.; Thurairatnam, Sukanthini:
1,3-Dipolar Cycloadditions to Unsymmetrical Ketone-Derived Chiral Stabilized Azomethine Ylides: Strategies for the Synthesis of Highly Substituted Amino Acids

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3279
Craig, Donald; King, N. Paul; Kley, Jörg T.; Mountford, David M.:
Heteroaromatic Decarboxylative Claisen Rearrangement Reactions

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3283
Hernandez-Juan, Felix A.; Xiong, Xin; Brewer, Sarah E.; Buchanan, David J.; Dixon, Darren J.:
A Stereoselective Oxy-Michael Approach to THP*-Protected β-Hydroxy Esters

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3287
Blake, Alexander J.; Gill, Christopher; Greenhalgh, Daniel A.; Simpkins, Nigel S.; Zhang, Fengzhi:
An Asymmetric Synthesis of (+)-Erysotramidine

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3293
Caldwell, John J.; Cameron, Iain D.; Christie, Steven D. R.; Hay, Alastair M.; Johnstone, Craig; Kerr, William J.; Murray, Anthony:
Total Synthesis of Japanese Hop Ether Using an Efficient Intramolecular Pauson-Khand Reaction

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3297
Herre, Stephan; Steinle, Wencke; Rück-Braun, Karola:
Synthesis of Photoswitchable Hemithioindigo-Based ω-Amino Acids and Application in Boc-Based Peptide Assembly

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3301
Marcos, I. S.; Pedrero, A. B.; Sexmero, M. J.; Diez, D.; García, N.; Escola, M. A.; Basabe, P.; Conde, A.; Moro, R. F.; Urones, J. G.:
Synthesis of ent-Halimanolides from ent-Halimic Acid

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3311
Chechik-Lankin, Helena; Marek, Ilan:
Preparation and Synthetic Transformation of Alkenyl Carbamates into Vinyl Zirconocene Derivatives

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3319
Quiclet-Sire, Béatrice; Zard, Samir Z.:
The Synthesis of 1,2,3-Triazoles from Nitroalkenes - Revisited

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3327
Díez, David; García, Pilar; Moro, R. F.; Marcos, Isidro S.; Basabe, Pilar; Garrido, Narciso M.; Broughton, Howard B.; Urones, Julio G.:
Vinylsulfones as Nucleophiles and Michael Acceptors in the Same Step: Stereoselective Synthesis of Amino Acid Precursors

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3335
Trost, Barry M.; Jiang, Chunhui; Hammer, Kristin:
Palladium-Catalyzed Ring Opening of Isoprene Monoxide with Nitrogen Nucleophiles - Asymmetric Synthesis of Branched Amino Sugars

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3346
Calvet, Géraldine; Blanchard, Nicolas; Kouklovsky, Cyrille:
Synthesis of Polysubstituted Pyrroles from Nitroso-Diels-Alder Cycloadducts

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3355
Abad, Antonio; Agulló, Consuelo; Cuñat, Ana C.; Navarro, Ismael:
Conversion of Alkyl Halides into Alcohols via Formyloxylation Reaction with DMF Catalyzed by Silver Salts

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3362
Koç, Fikret; Michalek, Florian; Rumi, Luigi; Bannwarth, Willi; Haag, Rainer:
Catalysts on Functionalized Polymer Chips (PC) as Recyclable Entities

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3373
Zhu, Bolin; Miljanić, Ognjen Š; Vollhardt, K. Peter C.; West, Michael J.:
Synthesis of 2,2′,3,3′-Tetramethyl- and 2,2′,3,3′-Tetra-tert-butylfulvalene: Attractive Platforms for Dinuclear Transition Metal Fragments, as Exemplified by (η⁵:η⁵-2,2′,3,3′-t-Bu₄C₁₀H₄)M₂(CO)_n (M = Fe, Ru, Os, Mo) and First X-ray Crystal Structures of Fulvalene Diiron and Diosmium Complexes

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3380
Manthorpe, Jeffrey M.; Szpilman, Alex M.; Carreira, Erick M.:
Scalable Synthesis of a Mycosamine Donor. Overcoming Difficult Reactivity in Allose Systems

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3389
Ramalho, Rui; Beignet, Julien; Humphries, Alexander C.; Cox, Liam R.:
Using a Temporary Silicon Connection in a Highly Stereoselective Synthesis of a New Class of Cyclic Allenylsilanes

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3398
Clark, J. Stephen; Baxter, Carl A.; Castro, José L.:
Synthesis of the Tricyclic Core of the Marine Natural Product Labiatin A

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3405
Page, Philip C. Bulman; Buckley, Benjamin R.; Appleby, Louise F.; Alsters, Paul A.:
Highly Efficient Catalysts for Epoxidation Mediated by Iminium Salts

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3412
López-Cobeñas, Alberto; Cledera, Pilar; Sánchez, J. Domingo; López-Alvarado, Pilar; Ramos, M. Teresa; Avendaño, Carmen; Menéndez, J. Carlos:
Microwave-Assisted Synthesis of 2,5-Piperazinediones under Solvent-Free Conditions

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3423
Bala, Kason; Hailes, Helen C.:
Nitrile Oxide 1,3-Dipolar Cycloadditions in Water: Novel Isoxazoline and Cyclophane Synthesis

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3428
Mühlthau, Friedrich; Bach, Thorsten:
Diastereoselective Friedel-Crafts Cyclization Reactions to 2-Substituted 1-Phenyl-1,2,3,4-tetrahydronaphthalenes

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3437
Liu, Yi; Saha, Sourav; Vignon, Scott A.; Flood, Amar H.; Stoddart, J. Fraser:
Template-Directed Syntheses of Configurable and Reconfigurable Molecular Switches
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3446
Griffith, Jeraime A.; Rowlands, Gareth J.:
The Synthesis of Novel 4-(Aminomethyl)oxazoline Ligands

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3451
Gil, Salvador; Parra, Margarita; Rodriguez, Pablo; Sotoca, Enrique:
New Synthesis of (±)-Sitophilate Using Carboxylic Acid Dianion Methodology - A Stereoselectivity Study

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3456
Rudbeck, Hans Christian; Johannsen, Ib; Nielsen, Ole; Ruhland, Thomas; Sommer, Michael Bech; Tanner, David; Dancer, Robert:
Gram-Scale Synthesis of N-Aryl- and N-Aryl-N′-methylpiperazines on a Novel, Water-Swellable, Oxethane-Linked Poly(ethylene glycol) High-Loading Resin

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3463
Leach, Andrew G.; Houk, K. N.; Davies, Ian W.:
The Origins of Periselectivity and Substituent Effects in Electrocyclizations of o-Nitrosostyrenes: A Computational Study

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3468
Xu, Chunli; Bartley, Jonathan K.; Enache, Dan I.; Knight, David W.; Hutchings, Graham J.:
High Surface Area MgO as a Highly Effective Heterogeneous Base Catalyst for Michael Addition and Knoevenagel Condensation Reactions

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