Synthesis

Issue 21 · November 2025

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Editorial
III
Oestreich, M.; Ackermann, L.; Berionni, G.:
Paul Knochel at 70
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Table of Contents
VI
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Review
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3031
Cossy, Janine:
Cross-Coupling Reactions Between Alkynyl Metals and (Pseudo)Halides Induced by Earth-Abundant Transition Metals (Mn, Fe, Co, Ni, Cu)

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3049
Tian, Huan; Fleming, Fraser F.:
Isocyanoalkenes: Occurrence, Syntheses, and Reactivity

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Short Review
Published as part of the Special Topic Dedicated to Prof. Paul Knochel
3094
Jana, Sayan K.; Maji, Biplab:
Nickel-Catalyzed Cross-Electrophile Coupling Reactions of Alcohols and Their Derivatives

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3105
Piccardi, Riccardo; Micouin, Laurent:
An Overview of the Direct Preparation of Organoaluminum Compounds

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3127
Arnaudy, Roxane; Djebbar, Faycel; Tintar, Adrien; Lefèvre, Guillaume:
Bis-Alkenyl Compounds from Group XIV Elements (Si, Ge, Sn): Synthesis, Reactivity, and Applications

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3147
Dupeux, Aurélien; Truchon, Alexis; Gentilini, Emilie; Michelet, Véronique:
Gold- and Platinum-Catalyzed Prins-Type [2+2+2]-Cycloadditions: From Original Methods to Applications

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3158
Collum, David B.:
An Accidental Synthetic Chemist

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Paper
Published as part of the Special Topic Dedicated to Prof. Paul Knochel
3179
Gao, M.-Y.; Durandetti, M.; Gosmini, C.:
Synthesis of Diarylmethanes by Cobalt-Catalyzed Reductive Cross-Coupling via Csp³–S Bond Activation

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3189
Ramos, Mariah Carol; Kawasaki, Tairin; Cabanero, David; Sandmeier, Tobias; Rovis, Tomislav:
Skeletal Rearrangement of Pyridine Derivatives via a Light-Induced Ring Expansion

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3197
Blanco-López, Ester; Sirvent, Ana; Lulli, Thomas; Merino, Pedro; Nájera, Carmen; Yus, Miguel; Foubelo, Francisco; Retamosa, María de Gracia; Sansano, José M.:
Deacetylative Protocol to Obtain Diastereoselectively α-Fluoro-β-amino-oxindoles via a Mannich-Type Reaction using Aliphatic N-tert-Butanesulfinyl Imines

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3205
Okuda, Jun; Ingram, Aaron; Wang, Dong:
Halide-Substituted Grubbs–Hoveyda Catalysts for Aqueous Ring-Closing Metathesis

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3211
Boussandel, Sirine; Erb, William; Roisnel, Thierry; Blot, Marielle; Hurvois, Jean-Pierre; Butler, Ian; Samarat, Ali; Mongin, Florence:
Hexafluoroisopropanol-Promoted Substitution Toward the Synthesis of Enantiopure Ferrocene Phosphines

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3227
Grimm, Joyce A. A.; List, Benjamin:
Asymmetric Prins Cyclizations of O-Prenylated Salicylaldehydes
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3233
Conrads, Christian; Eilers, Maverick; Hülsken, Noah; Langletz, Tim; Hoffmann, Alexander; Herres-Pawlis, Sonja:
Synthesis of Novel Guanidine-Schiff-Base Iron(III) and Zinc(II) Complexes

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3241
Lee, Paul; Eugene, Bill D.; Allais, Christophe; Singer, Robert A.; Morken, James P.:
Tetrahydronaphthalenes by Enantioselective Migratory Suzuki–Miyaura Cross-Coupling of meso Bis(Boronic Esters)

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3251
Siegmund, Torsten; S. Stephenson, David; Ofial, Armin R.; Mayer, Robert J.; Mayr, Herbert:
How Electrophilic Are Keteniminium Ions?

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3263
Knupe-Wolfgang, Paula; Hilt, Gerhard:
The Transformation of Alkyl- and Aryl-Sodium Reagents with Simple Amides for the Direct Synthesis of Ketones

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3273
Acuña-Bolomey, Emilio G. A.; Oestreich, Martin:
Nickel-Catalyzed Enantioconvergent C(sp³)–C(sp³) Cross-Coupling between α-Iodogermanes and Alkylzinc Reagents

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3283
Sánchez-Roa, David; Kocher, Jasmin; Tortajada, Andreu; Hevia, Eva:
Structurally Mapping Sodium-Mediated Synthesis of 1,4-Substituted Dihydropyridines: Nucleophilic Addition vs. Deprotonative Metalation

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3295
Liu, Chuanqi; Wang, Xiaoqian; Du, Zhao; Wang, Yilei; Peng, Zhihua:
Nickel-Catalyzed Reductive Cross-Coupling of Chlorobismuths with Aryl Halides

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3307
Prapapongpan, Pannaporn; Nelson, Kylee B.; Zakharov, Lev N.; Blakemore, Paul R.:
Ferrocene-Templated Synthesis of Fused Aminofulvenes: Elaboration of Chalaniline A and a Reversed Regioisomer via a Ferroceno[b]chromone

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3315
Du, Hong-Jian; Yin, Hao-Nan; Zhou, Yun; Chu, Xue-Qiang; Xu, Hao; Shen, Zhi-Liang:
Pd-Catalyzed Decarboxylative Couplings of Aryl Triazine Esters With Zinc Polyfluorobenzoates

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Published as part of the Special Topic Dedicated to Prof. Paul Knochel
3325
Del Vecchio, Antonio; Kamal, Fadwa; Rouen, Mathieu; Mauduit, Marc:
Photochemical Activation of Ruthenium Complexes Containing Unsymmetrical Unsaturated N-Heterocyclic Carbenes for Olefin Metathesis

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3334
Goldfuss, Bernd; Wang, Xiaochen; Sartakov, Denis:
Hydrogen-Bonding Cyclodiphosphazane Organocatalysts in Enantioselective Michael Additions

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3341
Luo, Donghao; Yuan, Hao; Nie, Changrui; Ge, Shulei; Li, Jie:
Nickel-Catalyzed Alkylcarbonylation of α-Trifluoromethyl-Substituted Styrenes via Selective Monodefluorinative Strategy

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3350
García, Lorena; Carrillo, Luisa; Reyes, Efraím; Uria, Uxue; Prieto, Liher; Vicario, Jose L.:
Organocatalytic Enantioselective Nitro-Vinylcyclopropane-Cyclopentene Rearrangement: Expanding the Reactivity of Donor–Acceptor Cyclopropanes

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3361
Petrini, Marino; Palmieri, Alessandro; Gheco, Elettra:
Continuous Flow Telescoped Synthesis of Benzofurans Starting from Nitroalkanes and O-Acetyl Salicylaldehydes

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3370
Joly, Nicolas; Kjellberg, Marianne; Bouchet, Alexis; Nicolas, Emmanuel; Cantat, Thibault; Anthore-Dalion, Lucile:
Water-Mediated Rhenium-Catalyzed Photodeoxygenation of Polyfunctional Organic N-Oxides

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3377
Dierenbach, Niklas; Waloch, Christoph; Bauer, Felix; Seiche, Wolfgang; Breit, Bernhard:
Synthesis of Symmetric and P-Stereogenic Self-Assembling Pyridone-Based Phosphorus Ligands

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3394
Zhang, Qingxin; Berro, Mahdi; Darcel, Christophe:
Iron Catalyst and Blue Light Partnership for Selective Desulfurization of Secondary and Primary Thioamides

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errata
e1
Oestreich, M.; Ackermann, L.; Berionni, G.:
Erratum - Editorial

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Synthesis

Paul Knochel at 70

Linked PDF of Table of Contents

Cross-Coupling Reactions Between Alkynyl Metals and (Pseudo)Halides Induced by Earth-Abundant Transition Metals (Mn, Fe, Co, Ni, Cu)

Isocyanoalkenes: Occurrence, Syntheses, and Reactivity

Nickel-Catalyzed Cross-Electrophile Coupling Reactions of Alcohols and Their Derivatives

An Overview of the Direct Preparation of Organoaluminum Compounds

Bis-Alkenyl Compounds from Group XIV Elements (Si, Ge, Sn): Synthesis, Reactivity, and Applications

Gold- and Platinum-Catalyzed Prins-Type [2+2+2]-Cycloadditions: From Original Methods to Applications

An Accidental Synthetic Chemist

Synthesis of Diarylmethanes by Cobalt-Catalyzed Reductive Cross-Coupling via Csp³–S Bond Activation

Skeletal Rearrangement of Pyridine Derivatives via a Light-Induced Ring Expansion

Deacetylative Protocol to Obtain Diastereoselectively α-Fluoro-β-amino-oxindoles via a Mannich-Type Reaction using Aliphatic N-tert-Butanesulfinyl Imines

Halide-Substituted Grubbs–Hoveyda Catalysts for Aqueous Ring-Closing Metathesis

Hexafluoroisopropanol-Promoted Substitution Toward the Synthesis of Enantiopure Ferrocene Phosphines

Asymmetric Prins Cyclizations of O-Prenylated Salicylaldehydes

Synthesis of Novel Guanidine-Schiff-Base Iron(III) and Zinc(II) Complexes

Tetrahydronaphthalenes by Enantioselective Migratory Suzuki–Miyaura Cross-Coupling of meso Bis(Boronic Esters)

How Electrophilic Are Keteniminium Ions?

The Transformation of Alkyl- and Aryl-Sodium Reagents with Simple Amides for the Direct Synthesis of Ketones

Nickel-Catalyzed Enantioconvergent C(sp³)–C(sp³) Cross-Coupling between α-Iodogermanes and Alkylzinc Reagents

Structurally Mapping Sodium-Mediated Synthesis of 1,4-Substituted Dihydropyridines: Nucleophilic Addition vs. Deprotonative Metalation

Nickel-Catalyzed Reductive Cross-Coupling of Chlorobismuths with Aryl Halides

Ferrocene-Templated Synthesis of Fused Aminofulvenes: Elaboration of Chalaniline A and a Reversed Regioisomer via a Ferroceno[b]chromone

Pd-Catalyzed Decarboxylative Couplings of Aryl Triazine Esters With Zinc Polyfluorobenzoates

Photochemical Activation of Ruthenium Complexes Containing Unsymmetrical Unsaturated N-Heterocyclic Carbenes for Olefin Metathesis

Hydrogen-Bonding Cyclodiphosphazane Organocatalysts in Enantioselective Michael Additions

Nickel-Catalyzed Alkylcarbonylation of α-Trifluoromethyl-Substituted Styrenes via Selective Monodefluorinative Strategy

Organocatalytic Enantioselective Nitro-Vinylcyclopropane-Cyclopentene Rearrangement: Expanding the Reactivity of Donor–Acceptor Cyclopropanes

Continuous Flow Telescoped Synthesis of Benzofurans Starting from Nitroalkanes and O-Acetyl Salicylaldehydes

Water-Mediated Rhenium-Catalyzed Photodeoxygenation of Polyfunctional Organic N-Oxides

Synthesis of Symmetric and P-Stereogenic Self-Assembling Pyridone-Based Phosphorus Ligands

Iron Catalyst and Blue Light Partnership for Selective Desulfurization of Secondary and Primary Thioamides

Erratum - Editorial