Synthesis

Issue 02 · January 2019

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table of contents
XIII
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review
303
Banerjee, Arghya; Lei, Zhen; Ngai, Ming-Yu: Acyl Radical Chemistry via Visible-Light Photoredox Catalysis FREE ACCESS

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334
Esguerra, Kenneth Virgel N.; Lumb, Jean-Philip: Cu(III)-Mediated Aerobic Oxidations

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short review
359
Ghosh, Manoj K.; Rajkiewicz, Adam A.; Kalek, Marcin: Organocatalytic Group Transfer Reactions with Hypervalent Iodine Reagents

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371
Singh, Kuldeep; Kulbir, Kulbir; Gupta, Tarang; Kaur, Rajneesh; Singh, Raman: Applications of Rozen’s Reagent in Oxygen-Transfer and C–H Activation Reactions

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384
Passador, Kevin; Thorimbert, Serge; Botuha, Candice: ‘Heteroaromatic Rings of the Future’: Exploration of Unconquered Chemical Space

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feature
399
Fritze, Lars; Riensch, Nicolas A.; Helten, Holger: Catalytic Si/B Exchange Condensation: A Green B–C Coupling Method That Provides Access to Monodisperse (Het)arylborane ‘Trimers’

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407
Hein, Julia; Klett, Jan: The Preparation of Tetramethyl 1,1′,3,3′-Ruthenocenetetracarboxylate and Tetramethyl 1,1′,3,3′-Osmocenetetracarboxylate, and a Simplified Synthesis for Tetramethyl 1,1′,3,3′-Ferrocenetetracarboxylate

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psp
414
Shirinian, Valerii Z.; Lonshakov, Ilya A.; Zakharov, Alexey V.; Lvov, Andrey G.; Krayushkin, Mikhail M.: Practical Deoxygenation of Oxazole N-Oxides by PCl₃/Collidine

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paper
421
Dussart, Jade; Deschamp, Julia; Monteil, Maelle; Gager, Olivier; Migianu-Griffoni, Evelyne; Lecouvey, Marc: A General Protocol for the Synthesis of H-α-Hydroxyphosphinates

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433
Cortés, Iván; Borini Etichetti, Carla M.; Girardini, Javier E.; Kaufman, Teodoro S.; Bracca, Andrea B. J.: Total Synthesis and Cytotoxic Activity of 6,8-Dimethoxy-1,3-dimethylisoquinoline Isolated from Ancistrocladus tectorius: A 6π-Azaelectrocyclization Approach

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441
Faúndez, Rodrigo; Castillo, Francisco; Preite, Marcelo; Schott, Eduardo; Zarate, Ximena; Manriquez, Juan Manuel; Molins, Elies; Morales-Verdejo, Cesar; Chávez, Ivonne: Novel and Convenient Synthesis of 2,7-Dialkyl-1,8-dihydro-as-indacenes

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450
Greve, Eric; Porter, Jacob D.; Dockendorff, Chris: DFT-Assisted Design and Evaluation of Bifunctional Amine/Pyridine-Oxazoline Metal Catalysts for Additions of Ketones to Unactivated Alkenes and Alkynes

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463
Sibiryakova, Anastasiya E.; Shiryaev, Vadim A.; Reznikov, Alexander N.; Kabanova, Anastasiya A.; Klimochkin, Yuri N.: Asymmetric Synthesis of Adamantyl GABA Analogues

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470
Singh, Anoop S.; Agrahari, Anand K.; Mishra, Nidhi; Singh, Mala; Tiwari, Vinod K.: An Improved N-Acylation of 1H-Benzotriazole Using 2,2′-Dipyridyldisulfide and Triphenylphosphine

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CIF File
477
Brondani, Patrícia Bulegon; Mittersteiner, Mateus; Voigt, Morgana Aline; Klinkowski, Bruna Heloisa; Riva Scharf, Dilamara; de Jesus, Paulo Cesar: Synthetic Versatility of Lipases: Application for Si–O Bond Formation and Cleavage

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486
Hausherr, Arndt; Zimmer, Reinhold; Reissig, Hans-Ulrich: Additions of Carbohydrate-Derived Alkoxyallenes to Imines and Subsequent Reactions to Enantiopure 2,5-Dihydropyrrole Derivatives

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500
Sonawane, Amol D.; Shaikh, Yunnus B.; Garud, Dinesh R.; Koketsu, Mamoru: Synthesis of Isoquinoline-Fused Quinazolinones through Ag(I)-Catalyzed Cascade Annulation of 2-Aminobenzamides and 2-Alkynylbenzaldehydes FREE ACCESS

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508
Lu, Zheng; Yang, Yong-Qing: Catalyst-Free Photodriven Reduction of α-Haloketones with Hantzsch Ester

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516
Zhou, Xiao-Yu; Chen, Xia: Na₂CO₃-Catalyzed N-Acylation of Indoles with Alkenyl Carboxylates

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522
Wang, Lingna; Ma, Tiancong; Qiao, Mingming; Wu, Qiangxian; Shi, Deqing; Xiao, Wenjing: Visible-Light Photoredox-Catalyzed Cascade Reaction for the Synthesis of Pyrrolo[2,1-a]isoquinoline-Substituted Phosphonates

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530
Trujillo-Lagunas, Michelle L.; Medina-Mercado, Ignacio; Zaragoza-Galicia, Ivann; Olivo, Horacio F.; Romero-Ortega, Moisés: A Synthesis of 4-Chloro-2-(trichloromethyl)pyrimidines and Their Study in Nucleophilic Substitution

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538
Yang, Qin; Lei, Xiaoli; Yin, Zhijian; Deng, Zhihong; Peng, Yiyuan: Copper-Catalyzed NaBAr₄-Based N-Arylation of Amines

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545
Xu, Wei; Hei, Yu-Yuan; Song, Jian-Lan; Zhan, Xin-Chen; Zhang, Xing-Guo; Deng, Chen-Liang: Copper(I)-Catalyzed Thiolation of C–H Bonds for the Synthesis of Sulfenyl Pyrroles and Indoles

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552
Ahn, Sungwan; Yoon, Jeong A; Han, Young Taek: Total Synthesis of the Natural Pyridocoumarins Goniothaline A and B

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557
Zhou, Qiaoxia; Pan, Rihuang; Shan, Huanyu; Lin, Xufeng: Synthesis and Optical Resolution of 3,3,3′,3′-Tetramethyl-1,1′-spirobiindane-7,7′-diol

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564
Watts, Field M.; Bunce, Richard A.: Synthesis of Aryl-Substituted 3,3a,4,5-Tetrahydropyrrolo[1,2-a] quinolin-1(2H)-ones and 2,3,4,4a,5,6-Hexahydro-1H-pyrido[1,2-a]quinolin-1-ones

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573
Brand, George; Gomes, Carla M. B.; Costa, Willian F.; Foglio, Mary A.; Ruiz, Ana L. T. G.; Sarragiotto, Maria H.: Synthesis and Antitumor Activity of Novel 1-Substituted 3-(4,5-Substituted 1,2,4-Triazol-3-yl)-β-carboline Derivatives

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578
Stach, Guilherme; Peglow, Thiago J.; Roehrs, Juliano A.; Penteado, Filipe; Barcellos, Thiago; Jacob, Raquel G.; Lenardão, Eder J.; Perin, Gelson: Synthesis of 2-(Arylselanyl)benzo[b]chalcogenophenes via Intramolecular Cyclization of Vinyl Selenides

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