Synthesis

Issue 20 · October 2021

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table of contents
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review
3639
Laconsay, Croix J.; Tantillo, Dean J.:
Melding of Experiment and Theory Illuminates Mechanisms of Metal-Catalyzed Rearrangements: Computational Approaches and Caveats

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3653
de Gracia Retamosa, María; Döndaş, Haci Ali; Sobhani, Sara; Nájera, Carmen; Yus, Miguel A.; Sansano, José M.:
Photocatalytic Homocoupling Transformations

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short review
3673
Fershtat, Leonid L.; Teslenko, Fedor E.:
Five-Membered Hetarene N-Oxides: Recent Advances in Synthesis and Reactivity

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3683
Wang, Zhan-Yong; Guo, Qi; Xu, Shaohong; Wang, Kai-Kai:
Nucleophilic H-Phosphites, H-Phosphinates, and H-Phosphine Oxides in Organic Reactions

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3699
Ju, Guodong; Tu, Guanglian; Zhao, Yingsheng:
Recent Advances in Transition-Metal-Catalyzed Selective C–H Alkoxycarbonyldifluoromethylation Reactions of Aromatic Substrates

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3716
Li, Shen-Huan; Long, Cheng-Yu; Yang, Xin-Ge; Wang, Xue-Qiang:
Recent Progress in Amination Enabled by Transition-Metal-Free C(sp²)–O/C(sp²)–S Bond Cleavage Strategy

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feature
3725
Sedano, Carlos; Virumbrales, Cintia; Suárez-Pantiga, Samuel; Sanz, Roberto:
Aldol–Tishchenko Reaction of α-Oxy Ketones: Diastereoselective Synthesis of 1,2,3-Triol Derivatives

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3735
St-Gelais, Jacob; Giguère, Denis:
Protecting-Group-Free Synthesis of GB1107: An Orally Active Galectin-3 Antagonist

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3744
Zhu, Deng; Ye, Ai-Hui; Chen, Zhi-Min:
N-Selenocyanato-Dibenzenesulfonimide: A New Electrophilic Selenocyanation Reagent

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Supplementary Material

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3751
Zhu, Shaoqun; Wang, Jiawei; Zhou, Bing; Hou, Hong:
Copper/Di-tert-butyl Peroxide-Catalyzed Regioselective Hydroxyphosphorylation of 1,3-Enynes

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paper
3760
Trippe, Lukas; Nava, Analuisa; Frank, Andrea; Schollmeyer, Dieter; Nubbemeyer, Udo:
Synthesis of Enantiopure ω-(4-Fluorophenyl)-6,11-Methylene Lipoxin B₄ Methyl Ester

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3769
Dong, Bingbing; Lu, Jiansha; Bao, Honghao; Zhang, Yuanyuan; Liu, Yingguo; Leng, Yuting:
Copper-Catalyzed Sulfonylation of Cyclobutanone Oxime Esters with Sulfonyl Hydrazides

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3777
López-Mendoza, Pedro; Miranda, Luis D.:
α-Xanthylmethyl Ketones from α-Diazo ketones

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3791
Shchepochkin, Alexander V.; Chupakhin, Oleg N.; Demina, Nadezhda S.; Averkov, Maxim A.; Shimanovskaya, Tatyana Yu.; Slepukhin, Pavel A.; Volkov, Pavel A.; Telezhkin, Anton A.; Trofimov, Boris A.; Charushin, Valery N.:
Electrochemical Aromatization of Dihydroazines: Effect of Chalcogenophosphoryl (CGP) Substituents on Anodic Oxidation of 9-CGP-9,10-dihydroacridine

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3799
Zipfel, Pauline; Lalut, Julien; Sopková-de Oliveira Santos, Jana; Rochais, Christophe; Dallemagne, Patrick:
Aminothiaindanone as an Accessible Scaffold for a Three-Point Chemical Diversity

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3815
Zhang, Lanfei; Zhang, Xiaofei; Cui, Yongmei; Yang, Chunhao:
Direct Approach to 3-Fluoroindoles and 3,3-Difluoroindolines from 2,2-Difluoro-2-phenylethan-1-amines via C–H/N–H Coupling

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3827
Tsubaki, Kouta; Yamanaka, Tomoki; Hisamitsu, Takuya; Shimooka, Hirokazu; Kitamura, Mitsuru; Okauchi, Tatsuo:
New Phosphorylating Agents for the Synthesis of Phosphatidylethanolamines

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3836
Wang, Pengkai; Cao, Xuyan; Zhang, Songlin:
Applications of Ytterbium(II) Reagent as Grignard Reagent and Single-Electron Transfer Reagent in the Synthesis of 3-Substituted 2-Oxindoles

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3847
Wen, Chang; Wu, Chuan; Luo, Ruiqiang; Li, Qinghan; Chen, Feng:
Highly Efficient Synthesis of 2-Substituted Benzo[b]furan Derivatives from the Cross-Coupling Reactions of 2-Halobenzo[b]furans with Organoalane Reagents

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3862
Nakamura, Akira; Yamamoto, Kouhei; Murakami, Ryo; Kawashita, Norihito; Matsumoto, Kouichi; Maegawa, Tomohiro:
One-Pot Synthetic Approaches for the Construction of Isochroman-4-ones and Benzoxazin-3-ones Using O,P-Acetals

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errata
e4
Zhu, Shaoqun; Wang, Jiawei; Zhou, Bing; Hou, Hong:
Copper/Di-tert-butyl Peroxide-Catalyzed Regioselective Hydroxyphosphorylation of 1,3-Enynes

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Synthesis

Linked PDF of Table of Contents

Melding of Experiment and Theory Illuminates Mechanisms of Metal-Catalyzed Rearrangements: Computational Approaches and Caveats

Photocatalytic Homocoupling Transformations

Five-Membered Hetarene N-Oxides: Recent Advances in Synthesis and Reactivity

Nucleophilic H-Phosphites, H-Phosphinates, and H-Phosphine Oxides in Organic Reactions

Recent Advances in Transition-Metal-Catalyzed Selective C–H Alkoxycarbonyldifluoromethylation Reactions of Aromatic Substrates

Recent Progress in Amination Enabled by Transition-Metal-Free C(sp²)–O/C(sp²)–S Bond Cleavage Strategy

Aldol–Tishchenko Reaction of α-Oxy Ketones: Diastereoselective Synthesis of 1,2,3-Triol Derivatives

Protecting-Group-Free Synthesis of GB1107: An Orally Active Galectin-3 Antagonist

N-Selenocyanato-Dibenzenesulfonimide: A New Electrophilic Selenocyanation Reagent

Copper/Di-tert-butyl Peroxide-Catalyzed Regioselective Hydroxyphosphorylation of 1,3-Enynes

Synthesis of Enantiopure ω-(4-Fluorophenyl)-6,11-Methylene Lipoxin B₄ Methyl Ester

Copper-Catalyzed Sulfonylation of Cyclobutanone Oxime Esters with Sulfonyl Hydrazides

α-Xanthylmethyl Ketones from α-Diazo ketones

Electrochemical Aromatization of Dihydroazines: Effect of Chalcogenophosphoryl (CGP) Substituents on Anodic Oxidation of 9-CGP-9,10-dihydroacridine

Aminothiaindanone as an Accessible Scaffold for a Three-Point Chemical Diversity

Direct Approach to 3-Fluoroindoles and 3,3-Difluoroindolines from 2,2-Difluoro-2-phenylethan-1-amines via C–H/N–H Coupling

New Phosphorylating Agents for the Synthesis of Phosphatidylethanolamines

Applications of Ytterbium(II) Reagent as Grignard Reagent and Single-Electron Transfer Reagent in the Synthesis of 3-Substituted 2-Oxindoles

Highly Efficient Synthesis of 2-Substituted Benzo[b]furan Derivatives from the Cross-Coupling Reactions of 2-Halobenzo[b]furans with Organoalane Reagents

One-Pot Synthetic Approaches for the Construction of Isochroman-4-ones and Benzoxazin-3-ones Using O,P-Acetals

Copper/Di-tert-butyl Peroxide-Catalyzed Regioselective Hydroxyphosphorylation of 1,3-Enynes