Synfacts

Issue 06 · June 2008

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Synthesis of Natural Products and Potential Drugs
0551
Synthesis of Cassialoin FREE ACCESS

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0552
Synthesis of (-)-Perrottetinene

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0553
Synthesis of the Calcimimetic (+)-NPS R-568

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0554
Synthesis of Dysiherbaine

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0555
Formal Synthesis of (-)-Platensimycin

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0556
Synthesis of (-)-Salviasperanol

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0557
Synthesis of Chlorotonil A

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0558
Synthesis of Papaverine

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0559
Synthesis of (S,S)-Reboxetine

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0560
Formal Synthesis of Callipeltoside Aglycone

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0561
Synthesis of (3R,9R,10R)-Panaxytriol

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0562
Synthesis of Ouabain

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0563
Synthesis of Elatol

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0564
Synthesis of (-)-Erinacine E

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0565
Formal Synthesis (±)-Maritidine

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Synthesis of Heterocycles
0567
Stereoselective Synthesis of Hydroxypipecolic Acids

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0568
Electrochemically Induced Three-Component Synthesis of Chromenes

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0569
Three-Component Synthesis of 3,4,5-Trisubstituted Isoxazoles

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0570
Gallium(III) Triflate Catalyzed Conversion of Aldehydes and Ketones to Hydantoins

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0571
Intermolecular Zinc-Mediated Hydroamination of Alkynes to Indoles

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0572
Three-Component Synthesis of Highly Substituted 2-Imidazolines

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0573
Rhodium-Catalyzed Enantioselective Cycloaddition Route to Indolizidines FREE ACCESS

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0574
Synthesis of Acylaminopyrrolidines and -piperidines via Diastereoselective Ritter Reaction

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0575
Regioselective Two-Component Synthesis of Polysubstituted Pyrazoles

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0576
Gold(I)- and Silver(I)-Catalyzed Heteroannulation Route to Isoquinoline-N-Oxides

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0577
Acid-Base Catalyzed Formation of 2-Isoxazolines

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0578
Copper-Catalyzed Heteroannulation Route to Indolines

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0579
Synthesis of Quinazolinones by a Friedel-Crafts Heteroannulation Route

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0580
Metal-Free N-N Bond-Forming Route to Indazoles

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Synthesis of Materials and Unnatural Products
0581
New Routes to Siloles

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0582
Nanostructured Polymer Light-Emitting Diodes

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0583
C_3v-Symmetrical Calix[6]arenes

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0584
Subphthalocyanine-Based Donor-Acceptor System

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0585
Rhodamine Derivatives Get Redder with Silicon

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0586
Dyes with Double Color Modulation

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0587
Lighting-up Live Cells

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0588
A Spring-Loaded ROMPer FREE ACCESS

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0589
A Colorimetric Mercury Ion Sensor

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0590
Paratropic 20π Macrocycles

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0591
Bridge-Substituted Calix[4]arenes

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0592
High Electron Mobilities with Oligothiophenes Bearing Hexafluorocyclopentene

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0593
Excited-State Proton Cycle Produces Blue Luminescence

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
0595
Nickel-Catalyzed Hiyama Cross-Coupling Reaction of α-Bromo Esters

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0596
Rhodium-Catalyzed Reductive Aldol Reaction of Vinyl Ketones

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0597
Indium-Mediated Asymmetric Allylation of N-tert-Butanesulfinyl Imines

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0598
Amino Thioacetate Ligands for Enantioelective Aryl Transfers to Aldehydes

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0599
Cyclopropanation of Electron-Rich Olefins with Fischer Carbenes

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0600
Palladium-Catalyzed Dioxygenation of Alkenes

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0601
Enantioselective Cyanosilylation of Aldehydes Catalyzed by A Chiral Salen-Aluminum(III) Complex

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0602
Stereoselective Intermolecular Thiophosphinations of Terminal Alkynes

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0603
Heterobimetallic Catalyst for Intermolecular C-H Amination

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0604
Enantioselective Hydrosilylation of Ketones Catalyzed by Chiral Phosphine/Iron Complex

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0605
Enantioselective Niobium-Catalyzed Aza-Diels-Alder Reaction of Danishefsky’s Diene

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0606
Highly Diastereoselective Synthesis of Secondary and Tertiary Alcohols

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0607
Palladium-Catalyzed Double Phosphorylation of Alkynes

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0608
Asymmetric Simmons-Smith Reaction of Allylic Alcohols with Al(Salalen) Catalyst

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0609
Kinetic Resolution of Alcohols under Aerobic Conditions

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0610
Copper-Catalyzed Mukaiyama-Michael Reactions

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0611
BINOL-Titanium Catalyzed Hetero-Diels-Alder Reactions

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0612
Palladium-Catalyzed Enantioselective Synthesis of Allylic Thiol Derivatives

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0613
Kinetic Resolution of Homoallylic Alcohols by Retro-Allylation

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0614
Rhodium-Catalyzed [2+2+2] Cycloaddition of Carbodiimides

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0615
Applications of the Asymmetric Diels-Alder Reaction

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0616
Vanadium-Catalyzed Asymmetric Transcyanation of Aliphatic Aldehydes

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0617
Synthesis of Chiral α-Substituted Ketones via Enantioselective Protonation

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0618
Indium-Catalyzed syn-Addition of 1,3-Dicarbonyl Compounds

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0619
Enantioselective S_N2′ Allylic Alkylation Catalyzed by Chiral Diaminocarbene Complexes

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0620
Pd(II)-Catalyzed Cyclization of Allenyl Aldeydes with Arylboronic Acids

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0621
Synthesis of Highly Hindered β-Hydroxy Ketones and E-Enones

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0622
Aluminum(salalen)-Catalyzed Oxidation of Sulfides

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0623
Rhodium-Catalyzed Asymmetric Hydroboration

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Metal-Mediated Synthesis
0625
One-Pot Preparation of Hydroxyaryl- and (Hydroxyalkyl)aryltrifluoroborates FREE ACCESS

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0626
Anionic N-Fries Rearrangement Induced by I-Mg Exchange

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0627
Chemoselective O-Acylation of Aminoalcohols Catalyzed by a Zinc Cluster

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0628
Conversion of Amides into 2,2-Disubstituted Amines

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0629
Iron-Catalyzed S-Arylation of Thiols

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0630
Naphthalenes via Gold-Catalyzed Migration-Benzannulation Cascade

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0631
α-Arylation of Enaminones Using Organotrifluoroborates

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0632
Pd-Catalyzed α-Arylation of Oxindoles

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0633
Aziridination of Aliphatic Alkenes

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0634
Synthesis and Reactions of 1-Alkenyl-1,1-Heterobimetallic Reagents

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0635
Ketones from α-Oxocarboxylates by Decarboxylative Cross-Coupling

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0636
Conversion of a Vinyl Grignard Reagent to a 1,2-Dimetalated Ethane Synthon

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0637
Palladium-Catalyzed Methylation of Aryl C-H Bonds with Peroxides

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0638
Synthesis and Reactions of Aminoboranes

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Organo- and Biocatalysis
0639
Hydroamination of Nonactivated Alkenes FREE ACCESS

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0640
Enantioselective Baeyer-Villiger Oxidation of 3-Substituted Cyclobutanones

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0641
Bisphosphoric Acid - An Intriguing Catalyst Motif

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0642
Catalytic Asymmetric Phase-Transfer Hydroxylation of Oxindoles

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0643
Direct Asymmetric Iodination of Aldehydes

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0644
Cooperative Brønsted Acid Catalysis

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0645
A New Chiral Carbene Catalyst

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0646
An Organocatalytic Approach to Naphthoquinone Derivatives

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0647
Asymmetric Aldol Reaction Using New Bispidine Catalysts

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0648
Access to γ²-Amino Acids

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Polymer-Supported Synthesis
0649
Solid-Supported Cross-Metathesis

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0650
Preparation of Polyethylenes End-Tethered with POSS FREE ACCESS

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0651
Palladium Nanoparticles Supported onto Ionic Carbon Nanotubes FREE ACCESS

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0652
Suzuki-Miyaura Coupling Using Pd(OAc)₂ Immobilized on Reversed-Phase Alumina

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0653
Selective C3-Arylation of Free NH-Indoles with Pd-Modified Zeolite

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0654
Immobilization of Palladium Nanoparticles on Urea-MCF

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0655
The Solid-Phase Preparation of Biphenyltetrazoles via Suzuki Coupling

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0656
Conjugate Addition of Indoles Using ILIS-SO₂Cl Catalyst

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0657
Solid-Phase Synthesis of Tetrasubstituted 2-Imino-1,3-thiazolines

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0658
Oxidation of Alcohols Using Carbon-Supported Copper-Manganese Oxide

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0659
Combinatorial Library of Biaryl-Based Sulfonamides

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0660
Dithiane Hydrolysis by a Polymer-Supported Iodate

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0661
Dehydrogenation with SiO₂-Supported Iridium Catalysts

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0662
Hydrogenation with a Pd/PSi-TiO₂ System in Capillary

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Addenda and Errata
0663
Polymeric Difluoromethylation Reagent

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