Synthesis

Issue 05/2024

de Souza, João H.; Vargas, Jorge A. M.; Burtoloso, Antonio C. B.: An Improved Protocol for the Synthesis of Carbonyl Sulfoxonium Ylides

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Issue 02/2024

Espinoza-Hicks, José C.; Zaragoza-Galán, Gerardo; Camacho-Dávila, Alejandro A.: A Practical Synthesis of Homoallylic Diene Halides: Versatile Synthons for the Preparation of the Taxane A-Ring System

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Issue 24/2023

Chacon-Teran, Miguel A.; Bhattacharjee, Shubhra; Bailoo, Jeremy D.; Deonarine, Amrika; Findlater, Michael: Improved Syntheses of an Arseno-Fatty Acid (As-FA 362) and an Arseno-Hydrocarbon (As-HC 444)

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Issue 23/2023

Vorasin, Onanong; Phumjan, Tanawat; Saepua, Siriporn; Iwaniuk, Daniel; Kamchonwongpaisan, Sumalee; Yuthavong, Yongyuth; Thongpanchang, Chawanee; Srimongkolpithak, Nitipol: Development of a Practical Synthetic Method for Clinical Candidate 3-(2-{3-[(2,4-Diamino-6-ethylpyrimidin-5-yl)oxy]propoxy} phenyl)propanoic acid (P218) and Its Hydroxylated Metabolites

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Issue 20/2023

Broudic, Nathan; Pacheco-Benichou, Alexandra; Fruit, Corinne; Besson, Thierry: Synthesis of Trifunctional Thiazole-Fused Anthranilonitrile and Anthranilic Acid Derivatives

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Issue 17/2023

Saito, Katsuya; Sawazaki, Tomoya; Furusawa, Osamu; Kosugi, Teruo; Kimura, Yoshikazu; Kirihara, Masayuki: Practical Synthesis of Pent-4-yn-1-ol and Pent-4-en-1-ol from Tetrahydrofurfuryl Halides

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Issue 16/2023

Liu, Zheng; Lu, Sheng-Mei; Zhao, Bao-Qian; Chen, Hao-Dong; Chen, Mu-Wang; Zhou, Yong-Gui: An Improved Synthesis of Chiral 2,2′-Bipyridine Ligand C3-ACBP Without Column Chromatography

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Issue 14/2023

Weber, T. Moritz; Pietruszka, Jörg: Synthesis of a Water-Soluble Tridentate (Dimethylamino)ethyl Cu(I)/Cu(II)-Ligand

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Issue 13/2023

Sugiishi, Tsuyuka; Motegi, Ryohei; Amii, Hideki: Intramolecular Cyclization of N-Propargylic Amides without Transition-Metal Catalysis for Synthesis of Fluoroalkylated Oxazoles: Using Carboxylic Acid Anhydrides as the Fluoroalkyl Source

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Issue 23/2022

Hebert, Olivier; Dubouilh-Benard, Carole; Campos, Joana F.; Berteina-Raboin, Sabine; Fruit, Corinne; Besson, Thierry: Monitoring of Catalyst-Free Microwave-Assisted MCR-Type Synthesis of 2-Amino-3-cyano-4H-chromene Derivatives Using Raman Spectrometry

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Issue 11/2022

Peshkov, Anatoly A.; Makhmet, Azat; Bakulina, Olga; Kanov, Evgeny; Gainetdinov, Raul; Peshkov, Vsevolod A.; Dar’in, Dmitry; Krasavin, Mikhail: A General Approach to Spirocyclic Piperidines via Castagnoli–Cushman Chemistry

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Issue 10/2022

Hayward, John J.; Mader, Lavleen; Trant, John F.: Giving Preparative Thin-Layer Chromatography Some Tender ­Loving Care

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Issue 07/2022

Müller, Harald; Bourcet, Léa: [1,3]-Dithiolo-[4,5-d][1,3-dithiole]-2,5-dione

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Issue 03/2022

Alterman, Joshua L.; Kraus, George A.: A Convenient Procedure for Sonogashira Reactions Using Propyne

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Issue 02/2022

Janicki, Ignacy; Kiełbasiński, Piotr: A Straightforward, Purification-Free Procedure for the Synthesis of Ando and Still–Gennari Type Phosphonates

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Issue 23/2021

Nizovtsev, Alexey V.; Bovin, Nicolai V.: A Facile Synthesis of 2-Aminopropane-1,2,3-tricarboxylic Acid and Its Symmetrical Dimethyl Ester

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Issue 19/2021

Kadyrov, Renat; Tok, Oleg L.: Convenient Synthesis of (R)-3-[(tert-Butoxycarbonyl)amino]piperidine and (R)-3-[(tert-Butoxycarbonyl)amino]azepane

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Issue 15/2021

Erb, William; Wen, Min; Roisnel, Thierry; Mongin, Florence: Synthesis of Ferrocenesulfonyl Chloride: Key Intermediate toward Ferrocenesulfonamides

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Issue 04/2021

Lei, Peng; Li, Guangchen; Ling, Yun; An, Jie; Nolan, Steven P.; Szostak, Michal: Protocol for Palladium/N-Heterocyclic Carbene-Catalyzed Suzuki–Miyaura Cross-Coupling of Amides by N–C(O) Activation

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Issue 24/2020

Moriguchi, Kento; Kono, Taro; Seko, Shinzo; Tanabe, Yoo: Gram-Scale Robust Synthesis of 1-Chloro-2,3-dimethyl-4-phenylnaphthalene: A Promising Scaffold with Three Contiguous Reaction Positions

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Issue 23/2020

Bhilare, Shatrughn; Kori, Santosh; Shet, Harshita; Balaram, Gundapally; Mahendar, Koosam; Sanghvi, Yogesh S.; Kapdi, Anant R.: Scale-Up of a Heck Alkenylation Reaction: Application to the Synthesis of an Amino-Modifier Nucleoside ‘Ruth Linker’

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Issue 22/2020

Delpe Acharige, Anjana; Neri, Raul; Hodgson, James; Bossmann, Stefan H.: A Catalyst-Free, Temperature-Driven One-Pot Synthesis of 1-Adamantylhydrazine Hydrochloride

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Issue 21/2020

Kadari, Lingaswamy; Roisnel, Thierry; Erb, William; Krishna, Palakodety Radha; Mongin, Florence: Remote Deprotometalation-Iodolysis of N,N-Diisopropyl-2-trimethylsilylferrocenecarboxamide: A New Route Toward 1,1′-Disubstituted Ferrocenes

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Issue 20/2020

Souquet, Florence; Drici, Wassila; Fayssal, Sandra Abi; Lazouni, Imane; Thueillon, Sébastien; Pérard-Viret, Joëlle: N-Acyliminium Ion Chemistry: Improving the Access to Unsaturated γ-Lactams and Their N-α-Methoxylated Derivatives: Application to an Expeditive Synthesis of (±)-Crispine A

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Issue 19/2020

Cavarischia, Claudia; Comely, Alex; Écija, Marta; Iacoangeli, Tommaso; Pastó, Mireia; Silvestri, Lavinia; Furlotti, Guido: A Convenient, Scalable Process for the Preparation and Purification of Calcium Acamprosate

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Issue 18/2020

Zisopoulou, Stavroula A.; Pafili, Anastasia E.; Gkizis, Petros; Andreou, Thanos; Koftis, Theoharis V.; Lithadioti, Alexandra; Neokosmidis, Efstratios; Gallos, John K.: Environmentally Benign Large-Scale Synthesis of a Precursor to Vortioxetine

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Issue 17/2020

Steinebach, Christian; Voell, Sabine Anna; Vu, Lan Phuong; Bricelj, Aleša; Sosič, Izidor; Schnakenburg, Gregor; Gütschow, Michael: A Facile Synthesis of Ligands for the von Hippel–Lindau E3 Ligase

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Issue 15/2020

Tom, Mai-Jan; Turnbull, Ben W. H.; Evans, P. Andrew: A Concise and Modular Three-Step Synthesis of (S)-Verapamil using an Enantioselective Rhodium-Catalyzed Allylic Alkylation Reaction

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Issue 08/2020

Mulks, Florian F.; Heckershoff, Robin; Zimmer, Marc; Hashmi, A. Stephen K.: Practical Preparation of Cyclopropenone 1,3-Propanediol Ketal

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Issue 06/2020

Morra, Barbora; Morra, Nicholas A.; MacDonald, Daniel G.; Pagenkopf, Brian L.: Gram-Scale Synthesis of the Co(nmp)₂ Catalyst to Prepare trans-2,5-Disubstituted Tetrahydrofurans by the Aerobic Oxidative Cyclization of Pent-4-en-1-ols

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Issue 05/2020

Sherwood, Alexander M.; Meisenheimer, Poncho; Tarpley, Gary; Kargbo, Robert B.: An Improved, Practical, and Scalable Five-Step Synthesis of Psilocybin

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Issue 23/2019

Zilate, Bouthayna; Fischer, Christian; Schneider, Lukas; Sparr, Christof: Scalable Synthesis of Acridinium Catalysts for Photoredox Deuterations

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Issue 20/2019

Ashida, Yuya; Kondo, Shoichi; Arashiba, Kazuya; Kikuchi, Takamasa; Nakajima, Kazunari; Kakimoto, Seizo; Nishibayashi, Yoshiaki: A Practical Synthesis of Ammonia from Nitrogen Gas, Samarium Diiodide and Water Catalyzed by a Molybdenum–PCP Pincer Complex

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Issue 17/2019

Erb, William; Roisnel, Thierry; Dorcet, Vincent: Practical Chromatography-Free Synthesis of 2-Iodo-N,N-diiso­propylferrocenecarboxamide and Further Transformations

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Issue 16/2019

Tao, Jason; Murphy, Graham K.: A Practical, Large-Scale Synthesis of p-(Difluoroiodo)toluene (p-TolIF₂)

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Issue 15/2019

Torruellas, Carilyn; Hsu, Fu-Lian; Walz, Andrew J.: Synthesis of N-Pyridyl Hydroxylamines via Copper-Catalyzed Cross-Coupling

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Issue 13/2019

Yin, Lingfeng; Mao, Yongjun; Liu, Yaowei; Bu, Lehao; Zhang, Long; Chen, Wenxin: New Synthetic Route to Tucatinib

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Issue 12/2019

Rouzier, Florian; Sillé, Rosanne; Nourry, Arnaud; Tessier, Arnaud; Pipelier, Muriel; Guillarme, Stéphane: Practical Gram-Scale Synthesis of Either α- or β-Anomer of C-Vinyl Glycosides

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Issue 07/2019

Nakura, Ryo; Inoue, Kazuki; Okano, Kentaro; Mori, Atsunori: Practical Synthesis of Precursors of Cyclohexyne and 1,2-Cyclohexadiene

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Issue 04/2019

Morales-Chamorro, Maricela; Vázquez, Alfredo: A Facile Synthesis of N-Boc-azocan-5-one

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Issue 02/2019

Shirinian, Valerii Z.; Lonshakov, Ilya A.; Zakharov, Alexey V.; Lvov, Andrey G.; Krayushkin, Mikhail M.: Practical Deoxygenation of Oxazole N-Oxides by PCl₃/Collidine

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Issue 23/2018

Baidilov, Daler; Makarova, Mariia; Rycek, Lukas; Hudlicky, Tomas: Preparation of Rearranged Allylic Isocyanates from the Reaction of Allylic Alcohols with 1-Cyano-4-dimethylaminopyridinium Bromide

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Issue 17/2018

Olmos, Andrea; Pereira, Ana; Belderrain, Tomás R.; Pérez, Pedro J.: Multigram Synthesis of Thallium Trispyrazolylborate Compounds

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Fearraigh, Martin P. Ó; Matlock, Johnathan V.; Illa, Ona; McGarrigle, Eoghan M.; Aggarwal, Varinder K.: Synthesis of Isothiocineole and Application in Multigram-Scale Sulfur Ylide Mediated Asymmetric Epoxidation and Aziridination

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Issue 09/2018

Khan, Imran; Luo, Zhi-Bin; Valeru, Anil; Xu, Yin; Liu, Bin; Sangepu, Bhavanarushi; Xie, Ji-Min: Dihydroxylation of Olefins with Potassium Permanganate Catalyzed­ by Imidazolium Salt

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Issue 08/2018

Jiang, Xingguo; Ma, Shengming: Studies on Iron-Catalyzed Aerobic Oxidation of Benzylic Alcohols to Carboxylic Acids

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Issue 05/2018

Matoba, Kazutaka; Eizawa, Aya; Nishimura, Shunsuke; Arashiba, Kazuya; Nakajima, Kazunari; Nishibayashi, Yoshiaki: Practical Synthesis of a PCP-Type Pincer Ligand and Its Metal Complexes­

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Issue 04/2018

Plevová, Kristína; Mudráková, Brigita; Šebesta, Radovan: A Practical Three-Step Synthesis of Vinylferrocene

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Issue 02/2018

Buonomo, Joseph A.; Eiden, Carter G.; Aldrich, Courtney C.: Scalable Synthesis of Hydrido-Disiloxanes from Silanes: A One-Pot Preparation of 1,3-Diphenyldisiloxane from Phenylsilane

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Issue 24/2017

Hamper, Bruce C.; Sullivan, Brendan T.; Rath, Nigam P.; Spilling, Christopher D.: A Practical Gram-Scale Synthesis of Acrylohydroxamic Acid

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Issue 18/2017

Weiberth, Franz J.; Bourque, Andre J.; Elenbaas, Steven; Hanna, Reda; Powers, Matthew R.; Siegel, Craig S.; Zhao, Jin: Scalable Syntheses of Chirally Pure Mono-protected and Orthogonally Di-protected cis-3,4-Diaminotetrahydrofurans

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Issue 14/2017

Kotthaus, Andreas F.; Ballaschk, Frederic; Stakaj, Vjoni; Mohr, Fabian; Kirsch, Stefan F.: Synthesis and Resolution of a Chiral Diamine: 2,2′-(Propane-2,2-diyl)dipyrrolidine

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Issue 13/2017

Denmark, Scott E.; Chi, Hyung Min: Synthesis of 2-Alkenyl-Tethered Anilines

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Issue 11/2017

van der Haas, Richard N. S.; Dekker, Jeroen A.; Hassfeld, Jorma; Hager, Anastasia; Fey, Peter; Rubenbauer, Philipp; Damen, Eric: Synthesis and Properties of 2-Oxa-6-azaspiro[3.3]heptane Sulfonate Salts

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Issue 09/2017

De Angelis, Sonia; Celestini, Paolo; Rebuzzini, Gabriele; Degennaro, Leonardo; Luisi, Renzo: A Practical ¹¹B NMR Evaluation of BH₃ Titer in Commercial Solutions

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Issue 03/2017

Blades, Kevin; Glossop, Steven C.: A Three-Step Protocol towards N-8-(2,2-Dimethoxyethyl)-2-methylsulfanylpyrido[2,3-d]pyrimidin-7-one

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Issue 21/2016

Luo, Zhi-bin; Zhao, Chen; Xie, Jimin; Lu, Hong-fei: An Efficient and Practical Method for Olefin Dihydroxylation

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Issue 20/2016

Godeau, Julien; Martinet, Anthony; Levacher, Vincent; Fruit, Corinne; Besson, Thierry: Efficient Microwave-Assisted Synthesis of Methyl 4- or 5-Nitro­anthranilate

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Issue 18/2016

Zhu, Cheng-Liang; Lu, Deng-Fu; Sears, Jeffrey D.; Jia, Zhen-Xin; Xu, Hao: Practical Synthetic Procedures for the Iron-Catalyzed Intermolecular Olefin Aminohydroxylation Using Functionalized Hydroxylamines

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Issue 14/2016

Hill, Matthew D.: A Multicomponent Approach to Highly Substituted 1H-Pyrazolo[3,4-b]pyridines

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Issue 13/2016

Castillo-Rangel, Norma; Pérez-Díaz, José Oscar H.; Vázquez, Alfredo: An Expeditious Synthesis of 8-Methoxy-1-tetralone

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Issue 11/2016

Kerkovius, Jeff K.; Menard, Frederic: A Practical Synthesis of 6,8-Difluoro-7-hydroxycoumarin Derivatives for Fluorescence Applications

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Issue 09/2016

Mao, Yongjun; Zhu, Chunping; Zhu, Guoqing; Wang, Han; Ren, Xinfeng: Kilogram Synthesis of Crebinostat

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Issue 08/2016

Herrera, Alberto; Linden, Anthony; Heinemann, Frank W.; Brachvogel, René-Chris; von Delius, Max; Dorta, Romano: Optimized Syntheses of Optically Pure P-Alkene Ligands: Crystal Structures of a Pair of P-Stereogenic Diastereomers

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Issue 07/2016

Balakrishna, Bugga; Vidal-Ferran, Anton: A Practical Synthesis of Rhodium Precatalysts for Enantioselective Hydrogenative Transformations

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Issue 02/2016

Correia, Henrique D.; Cicolani, Renato S.; Moral, Raphael F.; Demets, Grégoire J. F.: Easy Synthesis of trans-4,5-Dihydroxy-2-imidazolidinone and 2,4-Dimethylglycoluril

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Issue 01/2016

Varjosaari, Sami E.; Suating, Paolo; Adler, Marc J.: One-Pot Synthesis of O-Aryl Carbamates

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Issue 24/2015

Beaudoin, Daniel; Rominger, Frank; Mastalerz, Michael: Efficient, Scalable Syntheses of Important Intermediates in Tribenzotriquinacene Chemistry

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Issue 23/2015

Roy, Sudeshna; Sutivisedsak, Nongnuch; Hamper, Bruce C.; Lyss, Alexander M.; Spilling, Christopher D.: A Practical and Scalable Synthesis of (S)- and (R)-1-(Dimethoxyphosphoryl)allyl Methyl Carbonates

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Issue 20/2015

Mao, Yongjun; Zhu, Chunping; Kong, Ziyang; Wang, Jiao; Zhu, Guoqing; Ren, Xinfeng: New Synthetic Process for Bosutinib

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Issue 18/2015

Zhang, Ziyang; Kitamura, Yoshiaki; Myers, Andrew G.: An Efficient Directed Claisen Reaction Allows for Rapid Construction of 5,6-Disubstituted 1,3-Dioxin-4-ones

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Issue 17/2015

Lei, Xiangyang; Jalla, Anusha; Abou Shama, Mhd A.; Stafford, Jamie M.; Cao, Billy: Chromatography-Free and Eco-Friendly Synthesis of Aryl Tosylates and Mesylates

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Issue 15/2015

Le Marquer, Nicolas; Laurent, Mathieu Yves; Martel, Arnaud: A Practical and Cost-Effective Method for the Synthesis of Bicyclo[2.2.2]octane-1,4-dicarboxylic Acid

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Issue 14/2015

Marelli, Enrico; Fernández Salas, José A.; Nolan, Steven P.: Synthesis of an Intermediate of Nafoxidine via Nickel-Catalyzed Ketone Arylation

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Issue 13/2015

Chmurski, Kazimierz; Stepniak, Pawel; Jurczak, Janusz: Improved Synthesis of C2 and C6 Monoderivatives of α- and β-Cyclodextrin via the Click Chemistry Approach

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Issue 11/2015

Aitken, R. Alan; Meehan, Anna; Power, Lynn A.: Synthesis of (R)-Lactic Acid and (2R,5R)-2-tert-Butyl-5-methyl-1,3-dioxolan-4-one

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Issue 10/2015

Mao, Yongjun; Jiang, Luobin; Chen, Tianyun; He, Haijun; Liu, Gang; Wang, Han: A New and Practical Synthesis of Vortioxetine Hydrobromide

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Issue 09/2015

Kurata, Kaoruko; Inoue, Kumiko; Nishimura, Kazuhiko; Hoshiya, Naoyuki; Kawai, Nobuyuki; Uenishi, Junichi: Synthesis of Optically Pure (R)- and (S)-Tetrahydroisoquinoline-1- and -3-Carboxylic Acids

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Issue 08/2015

Molnár, Katalin; Takács, László; Kádár, Mihály; Kardos, Zsuzsanna; Faigl, Ferenc: A Practical Route for the Preparation of Bis(2,2,2-trifluoroethyl) 2-Oxoalkylphosphonates

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Issue 07/2015

Castelló, Luis M.; Nájera, Carmen; Sansano, José M.; Larrañaga, Olatz; de Cózar, Abel; Cossío, Fernando P.: Enantioselective Synthesis of exo-4-Nitroprolinates from Nitro­alkenes and Azomethine Ylides Catalyzed by Chiral Phosphor­amidite·Silver(I) or Copper(II) Complexes

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Issue 03/2015

Tummatorn, Jumreang; Thongsornkleeb, Charnsak; Ruchirawat, Somsak; Thongaram, Phanida; Kaewmee, Benyapa: Convenient and Direct Azidation of sec-Benzyl Alcohols by Trimethylsilyl Azide with Bismuth(III) Triflate Catalyst

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Issue 01/2015

Daniels, David S. B.; Smith, Siobhan R.; Lebl, Tomas; Shapland, Peter; Smith, Andrew D.: A Scalable, Chromatography-Free Synthesis of Benzotetramisole

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