Synfacts

Issue 08 · August 2011

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Synthesis of (±)-Cycloclavine and (±)-5-epi-Cycloclavine

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Syntheses of Basiliolide B and C8-Epimer and Transtaganolides C and D

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0815
Synthesis of (+)-Lysergic Acid, (+)-Lysergol, and (+)-Isolysergol

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Synthesis of GSK1842799

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0817
Synthesis of Buprenorphine

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0818
Synthesis of DC-45-A2

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0819
Synthesis of Dimebolin

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0820
Synthesis of Lactodehydrothyrsiferol

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0821
Synthesis of P13K Inhibitors

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0822
Synthesis of Suvorexant

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Synthesis of Heterocycles
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0823
Effects of Addition Rate on the Synthesis of Pyridopyrimidinediones

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0824
FeBr₃-Mediated Heteroannulation Route to Yield N-Amino-3-Nitrile-Indoles

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0825
Gold-Catalyzed Heteroannulation Route of N-Allyl Ureas to Tricyclic Indolines FREE ACCESS

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0826
Synthesis of 2-Mercaptobenzothiazoles via Metal-Free Heteroannulation

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0827
Cu-Mediated Heteroannulation Route to 2-Thio-Substituted Benzothiazoles

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0828
Sythesis of Serotonin Antagonists Using an Intramolecular Diels-Alder Approach

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0829
Heteroannulation Route to Indoles from N-Aryl Enamines via C-H Activation

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0830
Pd-Catalyzed Heteroannulation Route to Substituted 5-Azaindoles

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0831
Gold-Catalyzed [2+2+1] Synthesis of 2,5-Disubstituted Oxazoles

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0832
Pd-Catalyzed Synthesis of Indoles via NH₃ Cross-Coupling-Alkyne Cyclization

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0833
AuCl₃-Catalyzed Synthesis of 5-Bromomethyl Oxazoles from Amino Acids

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0834
Synthesis of 3-Amino-4-fluoropyrazoles Using Selectfluor

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0835
Ruthenium-Catalyzed Synthesis of Complex Indolizidinones

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0836
Palladium-Catalyzed C-H Activation Route to Dibenzothiophenes

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0837
De Novo Ruthenium-Catalyzed Synthesis of 2-Pyridones

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Synthesis of Materials and Unnatural Products
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0839
Iridium-Catalyzed Direct Tetraborylation of Perylene Bisimides

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0840
Selective NIR-Absorbing Dyes FREE ACCESS

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0841
Merocyanines Made Easy

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0842
Multiple CA-CR Reactions

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0843
Tuning the Electronic Properties of Fullerene

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0844
Numbers of Substitutions to Order: 2, 4, 5, 6, or Polymer

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0845
A Radically Different Approach to the Synthesis of Bifluorenes

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0846
Conjugated Polymers for ^¹O₂ Sensing

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0847
It’s all about the Twist!

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0848
Methanofullerenes for Improved OPVs

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0849
Phenoxazine Dyes

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0850
Chirality Sensor Based on Non-Linear Transmittance Change

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0851
Porphyrin Stability and Absorption Red Shift via BODIPY Extension

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0853
Cooperative Transition-Metal and Chiral Brønsted Acid Catalysis FREE ACCESS

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Iridium-Catalyzed Enantioselective Allylic Dearomatization of Phenols

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0855
Copper-Catalyzed Asymmetric Allylic Alkylation with Organolithium Reagents FREE ACCESS

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0856
Asymmetric Hydrogenation of Heterocyclic Compounds

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0857
New Scaffold for Asymmetric Catalysis via Salen-Metal Complexes

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0858
Sulfoxide-Alkene Hybrid Ligands in Rhodium-Catalyzed 1,4-Addition

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0859
Palladium-Catalyzed Umpolung Allylation of Aldehydes

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0860
Enantioselective Propargylic Amination of Nonaromatic Propargylic Esters

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0861
Stereodivergent Asymmetric Reactions of α-Isothiocyanato Ester with Ketimines

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0862
Asymmetric Aza-Darzens Reaction Catalyzed by Mg Phosphate Salt

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0863
Synthesis of Chiral Furans by a Copper-Catalyzed Domino Process

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0864
Enantioselective Allylic Etherification

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0865
Asymmetric Epoxidations of Disubstituted Enones with Iron

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0866
Asymmetric Hydrocyanation of α,β-Unsaturated Ketones

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0867
Asymmetric Alkynylation of α-Trifluoromethyl Ketoimine Esters

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0868
Palladium-Catalyzed Asymmetric Hydrogenation of Enesulfonamides

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0869
Copper-Catalyzed 1,4-Addition of Organo-boronates to Alkylidene Cyanoacetates

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0870
Pd-Catalyzed Asymmetric Allylic Alkylation of Indoles and Pyrroles

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0871
Synthesis of Chiral Tetrahydrofurans by a Palladium-Catalyzed Cycloaddition

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0872
Diastereoselective 1,4-Addition of Asymmeric Lithium Amides

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0873
New Ligand for Zinc-Catalyzed Hydroxylation of β-Keto Esters and 1,3-Diesters

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0874
Gold- and Acid-Catalyzed Synthesis of Tetrahydropyrans and Tetrahydrofurans

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0875
Highly Selective Scandium-Catalyzed Aldehyde Crotylation

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0876
Ruthenium-Catalyzed Regio- and Enantio-selective Allylic Substitution with Water

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0877
Friedel-Crafts Alkylation of Indoles Catalyzed by a Chiral Palladium Complex

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0878
Asymmetric Domino Synthesis of N-Sulfonylamidines

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0879
Diastereoselective Ruthenium-Catalyzed [2+2] Cycloadditions of Allenenes

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0880
Silver-Catalyzed Asymmetric [3+2] Cycloaddition of Amino Esters to Olefins

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0881
Scandium-Catalyzed Asymmetric Sulfa-Michael Addition in Water

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0882
Asymmetric Addition of Arylboronic Acids to 2-Nitrostyrenes

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Metal-Mediated Synthesis
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0883
Highly Diastereoselective Additions to α-Silyloxy Ketones

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0884
Radical Alkylphosphanylation of Olefins

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0885
Amine-Directed Alkyl-Alkyl Suzuki Reactions FREE ACCESS

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0886
Palladium-Catalyzed Cyanomethylation of Aryl Halides

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0887
Room-Temperature Rh-Catalyzed Asymmetric Conjugate Addition

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0888
Synthesis of β-(Hydroxymethylaryl/alkyl)-α-methylene-γ-butyrolactones

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0889
Ni-Mediated Decarbonylative Cross-Coupling of Diorganozinc Reagents

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0890
Nickel-Catalyzed Cross-Coupling of Polyfluoroarenes with Arylboronic Acids

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0891
Pd-Catalyzed Chemoselective Cross-Couplings for Oligoarene Synthesis

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0892
Silyl Enol Ethers via Copper(II)-Catalyzed C-O Bond Formation

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0893
Ni-Catalyzed Cross-Coupling of Aryltrimethylammonium Iodides

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0894
Novel Base-Free Oxidative Heck Reaction

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0895
Anthranilamide as Protecting and Directing Group for Arylboronic Acids

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0896
Iron-Catalyzed Stereospecific C-H Bond Activation

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0897
Ni-Catalyzed Cross-Couplings of Tertiary Alkyl Grignards and Aryl Bromides

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Organo- and Biocatalysis
z899
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0899
Chiral Lewis Base Assisted Brønsted Acids

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0900
Catalytic Asymmetric Aziridination of α,β-Unsaturated Aldehydes

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0901
Catalytic Asymmetric Dichlorination of Allylic Alcohols

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0902
Intermolecular Hydroacylation of Cyclopropenes

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0903
Assembly of Complex Molecules via Dearomatization-Catalytic Desymmetrization

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0904
Asymmetric Michael Addition of α-Substituted β-Keto Amides

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0905
Catalytic Asymmetric Synthesis of Trisub-stituted Aziridines

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0906
Catalytic Asymmetric Conjugate Addition of NaHSO₃ to Chalcones

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0907
Intramolecular Asymmetric α-Allylation of Aldehydes via SOMO Umpolung

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0908
Catalytic Asymmetric Henry Reaction of Isatins

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0909
Chiral Brønsted Acid Catalyzed N-Functional-ization of Indoles

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Polymer-Supported Synthesis
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0911
Flow Synthesis of Alkaloids

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0912
A Mesoporous Organosilica-Supported Organocatalyst

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0913
A Platinum Nanocatalyst Confined within Carbon Nanotubes FREE ACCESS

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0914
Aerobic Oxidation of Alcohols Using IL@SBA-15-TEMPO

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0915
Aerobic Oxidation of Alcohols with Fe₃O₄/SiO₂-Supported TEMPO in Water

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0916
Magnetic Nanoparticle Supported Osmium for Olefin Dihydroxylation

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0917
NHPI/Fe(BTC)-Catalyzed Aerobic Oxidation of Alkanes

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0918
C-C Bond-Forming Reactions in Water with Pd-PPh₂-MSN

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0919
Mizoroki-Heck Reaction of Hypervalent Iodine with Pd Nanocatalyst

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0920
Chemoselective Hydrogenation with Pd Nanoparticle Cored Dendrimer

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0921
Suzuki-Miyaura Coupling with Nanoporous Metallic Glass Pd

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0922
Ionic Liquid Supported Synthesis of Benzimidazolones

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0923
Chiral MOF for Carbonyl-Ene and Hetero-Diels-Alder Reactions

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0924
Reductive N-Alkylation of Nitroarenes with Alcohols Catalyzed by Au/Fe₂O₃

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